PENINGKATAN SUHU KRITIS PADA SINTESIS BAHAN SUPERKONDUKTOR MAGNESIUM DIBORIDA DENGAN VARIASI UKURAN PARTIKEL SERBUK MG

Satrio Herbirowo, A. H. Yuwono, E. P. Utomo, Syafrizal Syafrizal, Agung Imaduddin
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Abstract

Studying the evolution of the MgB2 superconductor manufacturing process to improve critical temperature is important. The solid-state approach was used in this work to create a low-cost MgB2 superconductor. Variations in the purity of Boron were used as control parameters to evaluate the impact of dry milling on the production of the MgB2 bulk and low-temperature electrical properties. A 2:1 stoichiometric ratio of magnesium and boron powder was weighed and ground for 30 minutes. The ground powder was compressed and sintered for one hour at 1073 K. We were able to confirm through XRD and SEM research that the small particle size improved the MgB2 phase fraction and increase crystallite size in the production of the MgB2 sample. At 1073 K and 200 um of Mg, the sample sintered produced an MgB2 phase of 99.3%. The critical onset temperature (Tc-offset) improved from 39 to 40K, respectively.
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通过改变毫克粉粒度提高合成二硼化镁超导材料的临界温度
研究 MgB2 超导制造工艺的演变以提高临界温度非常重要。本研究采用固态方法制造低成本的 MgB2 超导体。硼纯度的变化被用作控制参数,以评估干磨对 MgB2 块体生产和低温电特性的影响。称取 2:1 的镁粉和硼粉,研磨 30 分钟。我们通过 XRD 和 SEM 研究证实,在生产 MgB2 样品的过程中,小粒径改善了 MgB2 的相分数并增加了晶粒尺寸。在 1073 K 和 200 um 的镁含量下,烧结样品生成的 MgB2 相占 99.3%。临界起始温度(Tc-offset)分别从 39K 提高到 40K。
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