Laboratory-scale extraction of Hildegardia barteri (Mast.) Kosterm. seed oil with different solvents, purified with membrane filtration

A. E. Adeniyi, J. O. Aremo, A. O. Oluwadare, S. Upendra
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Abstract

Abstract The shortcomings encountered from the use of conventional methods of refining draw considerable attention when it comes to the processing of edible oils. The present invention to this effect is the usage of membrane technology, which stands out as a suitable alternative, as it offers significant advantages such as minimal chemical additions, low energy consumption, and the retention of nutrients and other desired components. This paper seeks to ascertain the quality of edible oil extracted by different solvents, refined via membrane filtration. Amounts of 25 mL of crude oil sample were extracted with three different solvents (n-hexane, ethanol, and n-hexane-ethanol blend) from seeds of Hildegardia barteri (Mast.) Kosterm. and were refined using a micro-filter of pore size of 0.45 µm and an ultrafiltration membrane with 50 kDa cut off before bleaching and deodorizing to obtain table oil. Proximate composition and elemental analyses were carried out on the table oil samples produced and compared with food-grade standards. Results obtained showed 0.133–0.53% moisture content, 0.04% ash, 98.90–99.67% ether extract, 0.23% carbohydrate, and elemental compositions of 51.60–55.00% C, 6.12–6.30% H, 6.21–6.28% O, 0.01–0.02% N, and 13.0–15.0% P for edible oil samples. The findings of this study indicate that edible oil produced from the seeds of H. barteri via membrane technology yields good-quality oil for commercial production, except for the need to enhance further reduction of phosphorus content.
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用不同溶剂在实验室规模提取 Hildegardia barteri (Mast.) Kosterm.
摘要 在加工食用油时,使用传统精炼方法所遇到的缺陷引起了人们的极大关注。为此,本发明采用了膜技术,该技术具有化学添加物少、能耗低、可保留营养成分和其他所需成分等显著优点,是一种合适的替代方法。本文试图确定用不同溶剂萃取并通过膜过滤精炼的食用油的质量。从 Hildegardia barteri (Mast.) Kosterm.的种子中用三种不同的溶剂(正己烷、乙醇和正己烷-乙醇混合物)萃取了 25 mL 的粗油样品,并使用孔径为 0.45 µm 的微过滤器和截留分子量为 50 kDa 的超滤膜进行精制,然后进行漂白和除臭处理,得到食用油。对生产出的食用油样品进行了近似成分和元素分析,并与食品级标准进行了比较。结果显示,食用油样品的水分含量为 0.133-0.53%,灰分含量为 0.04%,醚提取物含量为 98.90-99.67%,碳水化合物含量为 0.23%,元素组成为 51.60-55.00%C、6.12-6.30%H、6.21-6.28%O、0.01-0.02%N 和 13.0-15.0%P。这项研究结果表明,通过膜技术从巴旦木种子中生产食用油,除了需要进一步降低磷含量外,还能生产出高质量的食用油,可用于商业生产。
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