Er, Cr: YSGG, Nd: YVO4, and Ti: Sapphire Lasers for Surface Treatment of Hybrid Ceramics on Bond Durability, Surface Texture, and Debonding to Resin Cement: A Scanning Electron Microscopy (SEM) Analysis

M. Alrabiah, Hanan Alsunbul, Basil Almutairi, Mohammad Aljanakh, Khaled M. Alzahrani, T. Abduljabbar
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Abstract

Aims: To assess composite ceramics treated with Er, Cr: YSGG (ECL), Nd: YVO4, and Ti: Sapphire lasers to samples treated with hydrofluoric acid (HF) and silane (S) for shear bond strength (SBS) and surface roughness (Ra). Material and Methods: 60 disc-shaped HRC specimens. Surface conditioning techniques divided HRC-prepared discs into four groups. Samples in Group 1: HRC pretreated with normal 9.5% HF, Group 2: ECL, Group 3: Ti-Sapphire, Group 4: Nd: YVO4. The profilometer measured all ceramic discs’ average surface Ra. Universal testing machines tested the resin-ceramic interface SBS. Surface topography was assessed using SEM. Shear bond scores and Ra were compared using a one-way ANOVA. A Tukey’s post hoc test assessed several group comparisons. Results: Group 2 (Ti Sapphire Laser+S) samples scored highest in Ra and SBS. Group 4 Nd: YVO4+S had the lowest Ra and SBS values. HF 20 sec+S, (Ti Sapphire Laser+S), (ECL+S), and (Nd: YVO4+S) had comparable SBS and Ra values (p>0.05). Conclusion: Laser-conditioned hybrid ceramics Er, Cr: YSGG, Nd: YVO4, and Ti-Sapphire lasers have shear bond strength and surface roughness comparable to 9.6% hydrofluoric acid.
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Er、Cr:用于混合陶瓷表面处理的铒、铬、YSGG、钕、YVO4 和钛、蓝宝石激光器对粘接耐久性、表面纹理以及与树脂水泥脱粘的影响:扫描电子显微镜 (SEM) 分析
目的:评估用 Er、Cr:YSGG (ECL)、Nd: YVO4 和 Ti: Sapphire 激光处理的复合陶瓷与氢氟酸 (HF) 和硅烷 (S) 处理的样品的剪切结合强度 (SBS) 和表面粗糙度 (Ra)。材料与方法:60 个圆盘状 HRC 试样。 表面调节技术将热轧卷制备的圆盘分为四组。第 1 组:用普通 9.5% HF 预处理的 HRC,第 2 组:ECL,第 3 组:Ti-Sapphire,第 4 组:Nd: YVO4。轮廓仪测量了所有陶瓷盘的平均表面 Ra 值。万能试验机测试了树脂-陶瓷界面 SBS。使用 SEM 评估表面形貌。采用单因素方差分析比较剪切粘接得分和 Ra。采用 Tukey 后检验对几个组进行比较。结果如下第 2 组(钛蓝宝石激光+S)样品在 Ra 和 SBS 方面得分最高。第 4 组 Nd:YVO4+S 的 Ra 值和 SBS 值最低。HF 20 秒+S、(钛蓝宝石激光+S)、(ECL+S)和(钕:YVO4+S)的 SBS 和 Ra 值相当(p>0.05)。结论激光调节混合陶瓷 Er、Cr:YSGG、Nd:YVO4 和 Ti-Sapphire 激光混合陶瓷的剪切结合强度和表面粗糙度与 9.6% 的氢氟酸相当。
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