Powder degradation as a consequence of laser interaction: A study of SS 316L powder reuse on the laser directed energy deposition process

IF 17.7 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY Accounts of Chemical Research Pub Date : 2024-01-19 DOI:10.2351/7.0001093
J. Gutjahr, Milton Pereira, Jurandir Marcos Sá de Sousa, H. S. Ferreira, Anselmo Thiesen Júnior
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Abstract

The feedstock capture efficiency on powder laser directed energy deposition (L-DED) is becoming a big challenge in the industrial use of the L-DED process for the manufacturing of large-scale AM parts. The powder capture efficiency is dependent on process optimization and the toolpath. The current literature presents a vast range of usual powder efficiency, between 3% and 32% and in some specific cases exceeding 90%. In L-DED, the powder-gas jet stream interacts with the laser beam adding material locally onto the substrate. Part of this material is captured by the melt pool. The not captured material that is affected by the laser beam suffers degradation. In the literature, there is a lack of studies related to powder reuse in the L-DED process. This paper presents a comprehensive study on the consequence of laser interaction with SS 316L metal powder particles during the L-DED process using a range of different powder characterization techniques to assess the powder morphology, size distribution, chemical composition, followability, and density. The study was conducted within eight powder reuse cycles, without adding virgin material to the powder batch. Reduction of particle size distribution range, increase in circularity, and improvement in the powder flowability were identified as consequences of powder reuse. The result of laser interaction with particles was further explored by scanning electron microscopy, presenting the continuous modification of the particles across the eight reuse cycles. The oxygen content on the particles was also measured to access the O2 pick-up as a consequence of particle heating.
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激光相互作用导致的粉末降解:关于激光定向能沉积工艺中 SS 316L 粉末再利用的研究
粉末激光定向能沉积(L-DED)的原料捕获效率正成为工业化使用 L-DED 工艺制造大规模 AM 零件的一大挑战。粉末捕获效率取决于工艺优化和工具路径。目前的文献显示,通常的粉末效率范围很大,介于 3% 和 32% 之间,在某些特定情况下超过 90%。在 L-DED 中,粉末气流与激光束相互作用,在基底上局部添加材料。部分材料被熔池捕获。未被激光束捕获的材料则会发生降解。文献中缺乏与 L-DED 工艺中粉末再利用相关的研究。本文采用一系列不同的粉末表征技术,对 L-DED 工艺中激光与 SS 316L 金属粉末颗粒相互作用的后果进行了全面研究,以评估粉末形态、尺寸分布、化学成分、可随性和密度。这项研究是在八个粉末重复使用周期内进行的,没有在粉末批次中添加原始材料。研究发现,粉末重复使用会导致粒度分布范围缩小、圆度增加和粉末流动性改善。扫描电子显微镜进一步探究了激光与颗粒相互作用的结果,显示了颗粒在八个重复使用周期中的持续变化。此外,还测量了颗粒上的氧含量,以了解颗粒加热后的氧气吸收情况。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Accounts of Chemical Research
Accounts of Chemical Research 化学-化学综合
CiteScore
31.40
自引率
1.10%
发文量
312
审稿时长
2 months
期刊介绍: Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.
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