Influence of the Processing Parameters on the Microstructure and Mechanical Properties of 316L Stainless Steel Fabricated by Laser Powder Bed Fusion

IF 4.7 3区 材料科学 Q1 ENGINEERING, ELECTRICAL & ELECTRONIC ACS Applied Electronic Materials Pub Date : 2024-02-09 DOI:10.3390/jmmp8010035
Germán Omar Barrionuevo, J. Ramos-Grez, Xavier Sánchez-Sánchez, Daniel Zapata-Hidalgo, J. L. Mullo, S. Puma-Araujo
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Abstract

Complex thermo-kinetic interactions during metal additive manufacturing reduce the homogeneity of the microstructure of the produced samples. Understanding the effect of processing parameters over the resulting mechanical properties is essential for adopting and popularizing this technology. The present work is focused on the effect of laser power, scanning speed, and hatch spacing on the relative density, microhardness, and microstructure of 316L stainless steel processed by laser powder bed fusion. Several characterization techniques were used to study the microstructure and mechanical properties: optical, electron microscopies, and spectrometry. A full-factorial design of experiments was employed for relative density and microhardness evaluation. The results derived from the experimental work were subjected to statistical analysis, including the use of analysis of variance (ANOVA) to determine both the main effects and the interaction between the processing parameters, as well as to observe the contribution of each factor on the mechanical properties. The results show that the scanning speed is the most statistically significant parameter influencing densification and microhardness. Ensuring the amount of volumetric energy density (125 J/mm3) used to melt the powder bed is paramount; maximum densification (99.7%) is achieved with high laser power and low scanning speed, while hatch spacing is not statistically significant.
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加工参数对激光粉末床熔融制造 316L 不锈钢微观结构和机械性能的影响
金属添加剂制造过程中复杂的热动力学相互作用降低了所生产样品微观结构的均匀性。了解加工参数对所产生的机械性能的影响,对于采用和推广这项技术至关重要。本研究的重点是激光功率、扫描速度和舱口间距对通过激光粉末床熔融技术加工的 316L 不锈钢的相对密度、显微硬度和显微结构的影响。在研究微观结构和机械性能时,使用了多种表征技术:光学显微镜、电子显微镜和光谱仪。相对密度和显微硬度评估采用了全因子实验设计。对实验结果进行了统计分析,包括使用方差分析(ANOVA)来确定加工参数之间的主效应和交互作用,以及观察每个因素对机械性能的贡献。结果表明,扫描速度是对致密化和显微硬度影响最大的统计参数。确保用于熔化粉末床的体积能量密度(125 J/mm3)至关重要;高激光功率和低扫描速度可实现最大致密化(99.7%),而舱口间距在统计学上并不重要。
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来源期刊
CiteScore
7.20
自引率
4.30%
发文量
567
期刊介绍: ACS Applied Electronic Materials is an interdisciplinary journal publishing original research covering all aspects of electronic materials. The journal is devoted to reports of new and original experimental and theoretical research of an applied nature that integrate knowledge in the areas of materials science, engineering, optics, physics, and chemistry into important applications of electronic materials. Sample research topics that span the journal's scope are inorganic, organic, ionic and polymeric materials with properties that include conducting, semiconducting, superconducting, insulating, dielectric, magnetic, optoelectronic, piezoelectric, ferroelectric and thermoelectric. Indexed/​Abstracted: Web of Science SCIE Scopus CAS INSPEC Portico
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