The Effect of Bonding Temperature on the Microstructural and Mechanical Properties of Transient Liquid Phase Bonded Commercially Pure Ti Joint

IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Engineering and Performance Pub Date : 2024-02-20 DOI:10.1007/s11665-023-07813-9
Vahid Maleki, Sajad Shakerin, Seyyed Alireza Ziaei, Hamid Omidvar, Seyyed Ehsan Mirsalehi
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Abstract

Commercially pure Ti (AMS 4902) was joined using the transient liquid phase bonding technique. The joining process was implemented at various temperatures of 820, 860, 900, and 1000 °C for 90 min under a vacuum atmosphere of 7.99 Pa. The microstructural investigations were carried out comprehensively using scanning electron microscopy equipped with the EDS elemental detector. The mechanical properties were characterized using the microhardness and shear strength tests. Strength properties in terms of ultimate shear strength and ductility were presented as force-extension diagrams. The presence of eutectic intermetallics in the joint centerline indicated that isothermal solidification was not achieved at low bonding temperatures. However, the increase in temperature to 1000 °C resulted in a fully isothermal solidified joint. The elemental gradients between the bonding centerline and the base metal leveled off at high temperatures of 900 and 1000 °C, where the solubility of Ti increased in the Cu crystal structure. A higher hardness of 270 HV with a uniform gradient was also observed across the joint produced at high temperatures of 900 and 1000 °C. A combination of high strength and ductility was obtained for the samples fabricated at 900 and 1000 °C bonding temperatures.

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接合温度对瞬态液相接合商业纯钛接头微观结构和机械性能的影响
使用瞬态液相键合技术连接了市售纯钛 (AMS 4902)。在 7.99 Pa 的真空环境下,在 820、860、900 和 1000 °C 的不同温度下进行了 90 分钟的接合过程。机械性能采用显微硬度和剪切强度测试进行表征。极限剪切强度和延展性方面的强度特性以力-拉伸图的形式呈现。接合中心线存在共晶金属间化合物,这表明在低接合温度下无法实现等温凝固。然而,温度升高到 1000 ℃ 时,接头完全等温凝固。接合中心线和基体金属之间的元素梯度在 900 和 1000 ℃ 高温时趋于平稳,此时钛在铜晶体结构中的溶解度增加。在 900 和 1000 °C 高温下生产的接头硬度更高,达到 270 HV,且梯度均匀。在 900 ℃ 和 1000 ℃ 焊接温度下制作的样品兼具高强度和延展性。
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来源期刊
Journal of Materials Engineering and Performance
Journal of Materials Engineering and Performance 工程技术-材料科学:综合
CiteScore
3.90
自引率
13.00%
发文量
1120
审稿时长
4.9 months
期刊介绍: ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance. The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication. Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered
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