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Inverse Problem in the Stochastic Approach to Modeling of Phase Transformations in Steels during Cooling after Hot Forming 热成型后冷却期间钢材相变建模随机方法中的逆问题
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-29 DOI: 10.1007/s11665-024-10458-x
Danuta Szeliga, Jakub Foryś, Natalia Jażdżewska, Jan Kusiak, Rafał Nadolski, Piotr Oprocha, Maciej Pietrzyk, Paweł Potorski, Paweł Przybyłowicz

The motivation for this research was the need for a reliable prediction of the distribution of microstructural parameters in steels during thermomechanical processing. The stochastic model describing the evolution of dislocation populations and grain size, which considers the random phenomena occurring during the hot forming of metallic alloys, was extended by including phase transformations during cooling. Accounting for a stochastic character of the nucleation of the new phase is the main feature of the model. Steel was selected as an example of the metallic alloy and equations describing the nucleation probability were proposed for ferrite, pearlite and bainite. The accuracy and reliability of the model depends on the correctness of the determination of the coefficients corresponding to the specific material. In the present paper these coefficients were identified using the inverse analysis for the experimental data. Experiments composed constant cooling rate tests for cooling rates in the range 0.1-20 °C/s. The inverse approach to a nonlinear model is ill-conditioned and must be transferred into an optimization problem, which requires formulating the appropriate objective function. Since the model is stochastic, it was a crucial, yet demanding task. The objective function based on a metric of the distance between measured and calculated histograms was proposed to achieve this goal. The original stochastic approach to identifying the phase transformation model for steels was tested, and an appropriate optimization strategy was proposed.

这项研究的动机是需要可靠地预测钢在热机械加工过程中的微观结构参数分布。描述位错群和晶粒大小演变的随机模型考虑了金属合金热成型过程中发生的随机现象,并通过将冷却过程中的相变纳入模型进行了扩展。该模型的主要特点是考虑了新相成核的随机性。以钢为例,提出了铁素体、波来石和贝氏体的成核概率方程。模型的准确性和可靠性取决于确定与特定材料相对应的系数的正确性。本文通过对实验数据进行反分析,确定了这些系数。实验包括冷却速率在 0.1-20 °C/s 范围内的恒定冷却速率测试。非线性模型的逆分析方法条件不完善,必须转换为优化问题,这就需要制定适当的目标函数。由于模型是随机的,因此这是一项关键而艰巨的任务。为了实现这一目标,我们提出了基于测量直方图和计算直方图之间距离度量的目标函数。对确定钢材相变模型的原始随机方法进行了测试,并提出了适当的优化策略。
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引用次数: 0
Effects of Defects and Shot Peening on Fatigue Properties of Additively Manufactured CoCrFeNiTiMo-Based High-Entropy Alloys 缺陷和喷丸强化对添加制造的钴铬镍钛钼基高熵合金疲劳性能的影响
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-19 DOI: 10.1007/s11665-024-10371-3
Miu Hayashi, Naoki Kurita, Tadatoshi Watanabe, Kenichi Yamamoto, Yuki Ogawa, Hiroyuki Akebono, Atsushi Sugeta

Recently, the automotive industry has increasingly focused on additive manufacturing as a new technology for reducing the weights of automobiles. In this study, fatigue tests were conducted on additively manufactured high-entropy alloys with different defect characteristics to clarify the relationships between their defect characteristics and fatigue strengths and to elucidate their fatigue fracture mechanisms. In addition, the effect of shot peening as an effective fatigue strength improvement method for an additively manufactured component was investigated. As a result, when defects formed by additive manufacturing were smaller than crystal grains, the numbers and sizes of defects affect fatigue crack growth behavior and barely affect fatigue life. Shot peening reduces the crack growth rate and is effective in extending the fatigue life. However, improvement in the fatigue limit is not achieved because the crack initiation site is a facet. From the above results, for defects smaller than the grain size, shot peening is a more effective method for improving fatigue life than reducing the numbers and sizes of defects.

最近,汽车行业越来越重视增材制造技术,将其作为减轻汽车重量的一项新技术。本研究对具有不同缺陷特征的增材制造高熵合金进行了疲劳试验,以明确其缺陷特征与疲劳强度之间的关系,并阐明其疲劳断裂机制。此外,还研究了喷丸强化作为一种有效的疲劳强度改进方法对快速成型部件的影响。结果表明,当增材制造形成的缺陷小于晶粒时,缺陷的数量和大小会影响疲劳裂纹的生长行为,几乎不会影响疲劳寿命。喷丸强化可降低裂纹生长率,并有效延长疲劳寿命。然而,由于裂纹起始点是一个面,因此无法改善疲劳极限。从上述结果来看,对于小于晶粒尺寸的缺陷,喷丸强化是比减少缺陷数量和尺寸更有效的提高疲劳寿命的方法。
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引用次数: 0
Investigating Optimum Hot Working Window of 2205 Duplex Stainless Steel Using Modified Dynamic Material Modeling
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-19 DOI: 10.1007/s11665-024-10099-0
Elvis M. Gonya, Mamookho E. Makhatha, Charles W. Siyasiya, Ndumiso M. Silubane, Ngeleshi M. Kibambe

This paper uses a modified dynamic material modeling (MDMM) suggested by Murty and Rao to develop processing maps (PM) of 2205 duplex stainless steels (DSS). Gleeble 1500D, a thermo-mechanical simulator was used to conduct single hit compression tests at a temperature between 850 and 1050 °C and strain rates of 0.001-5 s−1. Additionally hot compression tests at a strain rate of 15 s−1 and same temperature range were also conducted on a Bahr 805 dilatometer. As per general procedure acquired stress-strain data were corrected for friction and adiabatic heating, before constructing PMs at true strains of 0.1, 0.3, 0.5 and 0.8. Microstructures to validate the PM were prepared from safe domains and instability regimes belonging to PM of 0.8 true strain. Results showed that hot processing at intermediate to high strain rates and temperature leads to formation of flow instabilities such as mechanical twins and adiabatic shear bands. Safe domain located within the temperature range of (850-925) °C, strain rates of (2.6-15) s−1 and peak η = 35% gave an inhomogeneous microstructure with presumably non-uniform mechanical properties. This region was considered ideal for hot processing of 2205 DSS provided that deformation conditions are carefully controlled to optimise DRX. Low Z conditions also provided an optimum hot working for hot processing.

本文采用 Murty 和 Rao 提出的改良动态材料建模(MDMM)来绘制 2205 双相不锈钢(DSS)的加工图(PM)。使用热机械模拟器 Gleeble 1500D 在 850 至 1050 °C 温度和 0.001-5 s-1 应变速率下进行单击压缩试验。此外,还在 Bahr 805 膨涨仪上以 15 秒-1 的应变速率和相同的温度范围进行了热压缩试验。按照一般程序,在构建真实应变为 0.1、0.3、0.5 和 0.8 的 PM 之前,对获得的应力应变数据进行了摩擦和绝热加热校正。验证 PM 的微观结构是从安全域和属于 0.8 真实应变 PM 的不稳定状态制备的。结果表明,在中高应变率和温度下进行热加工会形成流动不稳定性,如机械孪晶和绝热剪切带。温度范围为 (850-925) ℃、应变率为 (2.6-15) s-1 和峰值 η = 35% 的安全域产生了一种不均匀的微观结构,其机械性能可能不均匀。该区域被认为是 2205 DSS 热加工的理想区域,前提是必须仔细控制变形条件以优化 DRX。低 Z 条件也为热加工提供了最佳热加工条件。
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引用次数: 0
Fracture Behavior of Hardfacing Alloy Coated Over Stainless Steel under Quasi-Static and Dynamic Loads
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-12 DOI: 10.1007/s11665-024-10389-7
Prince Joseph, M. Nani Babu, S. K. Albert

The fracture behavior of bi-material made of Ni-Cr-B-Si hardfacing alloy deposited over SS316LN substrate was evaluated under quasi-static and dynamic loads. The crack growth started from notch made on the deposit side and progress toward the substrate deposit interface under both loading conditions was monitored. The displacement rate in quasi-static loading and the loading rate for dynamic loading varied and crack propagation was studied. It was observed that the crack was deflected at the interface and not penetrated to the substrate, irrespective of loading conditions. The reason for crack deflection at the interface was analyzed using the energy-based method. It is shown that the ratio of fracture toughness of the interface to that of the substrate (0.044) is lower than the ratio of energy release rate for the deflecting crack to that of the penetrating crack (0.235). Thus, this material combination satisfies the condition for crack deflection rather than penetration. The fracture toughness of the interface was estimated as ~ 68 MPa m1/2 and it falls between that of hardfacing alloy and SS316LN base metal. Optical and SEM examinations were conducted to corroborate the crack path deviations during crack growth. Results suggest that isolated cracks might be present on hardfaced coatings on critical components for which such cracks are usually not permitted. It may be allowed in preference to repair of these cracks, which is difficult and significantly increases the risk of additional cracks forming on the deposits because of the high susceptibility of the hardfacing alloy to cracking.

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引用次数: 0
Assessment of Mechanical and Slurry Erosive Behavior on Laser-Textured Stainless Steel (SS410) 评估激光纹理不锈钢(SS410)的机械和泥浆侵蚀行为
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-12 DOI: 10.1007/s11665-024-10351-7
Mohit Vishnoi, Qasim Murtaza, Paras Kumar

In this paper, laser surface texturing (LST) has been used to create the circular and diamond shape texturing pattern on martensitic steel of grade SS410 to alter the various mechanical, surface, and tribological properties. The mechanical and surface characterizations have done on various shape-textured surfaces on SS410. Moreover, the slurry jet erosion test has performed on textured surfaces using a slurry erosion test rig. The hardness value of the various textured shape surface is higher than the others because mechanism of material removal for pattern is melting and evaporation, after applying an intense heat sudden cooling takes place. This might be altering the microstructure and enhances the hardness of the textured steel. The hardness value was the highest for circular-inward-textured case (HV0.3≈206) among all texturing. The tensile and flexural yield strength has marginally increased after texturing. The value of percentage elongation has marginally decreased after texturing. The modulus values for all the textured samples have enhanced as compared to untextured sample. Moreover, the modulus value of diamond-in textured samples are observed to be the highest i.e., ≈265GPa. The contact angles for all shapes of texturing patterns have greater values than untextured samples. All the textured surfaces show the hydrophobic and untextured surface as hydrophilic behavior. The outward textured surface has greater contact angle value (≈110°) as compared to others. The erosion resistance for the untextured samples have lesser among all textured samples, and the circular-in pattern has the highest erosion resistance. Because the erosion resistance is primarily depend on the hardness of the material, the plowing, microcutting lips, crater, and carbide pull-out type of wear mechanism has been identified using a scanning electron microscope.

本文采用激光表面纹理技术(LST)在 SS410 级马氏体钢上制作圆形和菱形纹理图案,以改变其各种机械、表面和摩擦学特性。对 SS410 的各种形状纹理表面进行了机械和表面特性分析。此外,还使用浆液侵蚀试验台对纹理表面进行了浆液喷射侵蚀试验。各种纹理形状表面的硬度值都高于其他表面,这是因为图案的材料去除机制是熔化和蒸发,在施加强热后会突然冷却。这可能会改变微观结构并提高纹理钢的硬度。在所有纹理中,圆形向内纹理的硬度值最高(HV0.3≈206)。纹理加工后,拉伸和弯曲屈服强度略有增加。纹理加工后,伸长率百分比值略有下降。与未纹理样品相比,所有纹理样品的模量值都有所提高。此外,金刚石纹理样品的模量值最高,为 ≈265GPa。与未纹理样品相比,所有形状纹理图案的接触角值都更大。所有纹理表面都表现为疏水,而未纹理表面则表现为亲水。与其他表面相比,外向纹理表面的接触角值较大(≈110°)。在所有纹理样品中,无纹理样品的抗侵蚀性较差,而圆弧形纹理样品的抗侵蚀性最高。由于抗侵蚀性主要取决于材料的硬度,因此使用扫描电子显微镜确定了犁、微切唇、凹坑和碳化物拉出等磨损机制。
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引用次数: 0
Effect of Ultrasonic Shot Peening on Surface Mechanical and Wear Behavior of Aluminum 7075-T651 Alloy
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-11-11 DOI: 10.1007/s11665-024-10352-6
Sudhir Behera, Ibrahim A. Alnaser, Gorti Janardhan, Pushpendra Kumar Dwivedi, Jayaprakash Murugesan, Anindya Basu, Asiful H. Seikh, Krishna Dutta

Aluminum alloys have gained widespread attention in various engineering sectors such as aerospace, automobile, and construction industries owing to their attractive properties. On the other hand, the tribological properties of aluminum alloys are of serious concern due to their limitation in terms of hardness. The objective of the current study was to enhance the surface mechanical properties including microhardness, compressive residual stress (CRS), and wear resistance of 7075-T651 aluminum alloy subjected to ultrasonic shot peening (USP). The samples of aluminum alloy were first treated with USP for various durations followed by different types of in-depth characterization. X-ray diffraction analysis was used to examine the bulk texture development after peening. The wear studies were carried out on a ball-on-plate wear testing machine under various applied loads. The results indicated an increase in hardness, surface roughness, and CRS of the samples with increasing USP time. Additionally, a marginal difference in the surface roughness of peened samples was observed for selected peening times. The wear depth and width of peened wear tracks were found to be less than those of un-peened ones. The surface tribological properties of the worn-out samples were studied using scanning electron microscopy (SEM). The elemental analysis was carried out using electron-dispersive spectroscopy (EDS).

{"title":"Effect of Ultrasonic Shot Peening on Surface Mechanical and Wear Behavior of Aluminum 7075-T651 Alloy","authors":"Sudhir Behera,&nbsp;Ibrahim A. Alnaser,&nbsp;Gorti Janardhan,&nbsp;Pushpendra Kumar Dwivedi,&nbsp;Jayaprakash Murugesan,&nbsp;Anindya Basu,&nbsp;Asiful H. Seikh,&nbsp;Krishna Dutta","doi":"10.1007/s11665-024-10352-6","DOIUrl":"10.1007/s11665-024-10352-6","url":null,"abstract":"<div><p>Aluminum alloys have gained widespread attention in various engineering sectors such as aerospace, automobile, and construction industries owing to their attractive properties. On the other hand, the tribological properties of aluminum alloys are of serious concern due to their limitation in terms of hardness. The objective of the current study was to enhance the surface mechanical properties including microhardness, compressive residual stress (CRS), and wear resistance of 7075-T651 aluminum alloy subjected to ultrasonic shot peening (USP). The samples of aluminum alloy were first treated with USP for various durations followed by different types of in-depth characterization. X-ray diffraction analysis was used to examine the bulk texture development after peening. The wear studies were carried out on a ball-on-plate wear testing machine under various applied loads. The results indicated an increase in hardness, surface roughness, and CRS of the samples with increasing USP time. Additionally, a marginal difference in the surface roughness of peened samples was observed for selected peening times. The wear depth and width of peened wear tracks were found to be less than those of un-peened ones. The surface tribological properties of the worn-out samples were studied using scanning electron microscopy (SEM). The elemental analysis was carried out using electron-dispersive spectroscopy (EDS).</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 23","pages":"13004 - 13018"},"PeriodicalIF":2.2,"publicationDate":"2024-11-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142789255","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancing the In Vitro Tribocorrosion Resistance of Titanium Alloy by Precipitation of Nano-Ti2Cu Phases
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-29 DOI: 10.1007/s11665-024-10121-5
Xiaoyan Wang, Yijing Gao, Mianmian Bao, Ying Liu, Lei Yang, Erlin Zhang

Compared with traditional Ti-based biomaterials, in recent years Cu-bearing titanium alloys have been considered among the most attractive metallic biomaterials for oral implants, owing to their excellent antibacterial properties. In this paper, the effects of the Cu content, the existing form of Cu element, and the oral environment on the tribocorrosion resistance of Ti-Cu alloys were investigated in comparison with pure titanium (cp-Ti). The results revealed that a low pH and (especially) a high fluoride ion concentration accelerated the tribocorrosion. The Ti-Cu alloys showed a higher tribocorrosion resistance than cp-Ti in all the simulated solutions tested, owing to the precipitation of nano-Ti2Cu during the aging treatment.

{"title":"Enhancing the In Vitro Tribocorrosion Resistance of Titanium Alloy by Precipitation of Nano-Ti2Cu Phases","authors":"Xiaoyan Wang,&nbsp;Yijing Gao,&nbsp;Mianmian Bao,&nbsp;Ying Liu,&nbsp;Lei Yang,&nbsp;Erlin Zhang","doi":"10.1007/s11665-024-10121-5","DOIUrl":"10.1007/s11665-024-10121-5","url":null,"abstract":"<p>Compared with traditional Ti-based biomaterials, in recent years Cu-bearing titanium alloys have been considered among the most attractive metallic biomaterials for oral implants, owing to their excellent antibacterial properties. In this paper, the effects of the Cu content, the existing form of Cu element, and the oral environment on the tribocorrosion resistance of Ti-Cu alloys were investigated in comparison with pure titanium (cp-Ti). The results revealed that a low pH and (especially) a high fluoride ion concentration accelerated the tribocorrosion. The Ti-Cu alloys showed a higher tribocorrosion resistance than cp-Ti in all the simulated solutions tested, owing to the precipitation of nano-Ti<sub>2</sub>Cu during the aging treatment.</p>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 23","pages":"12966 - 12975"},"PeriodicalIF":2.2,"publicationDate":"2024-10-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142789365","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Influence of Quenching and Partitioning Times on Austenite Stability and Tensile Properties of CMnAlSi Quenching and Partitioning Steel
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-23 DOI: 10.1007/s11665-024-10310-2
Chintada Umasankar, Apoorv Sobti, S. Sankaran, Uday Chakkingal

Quenching and partitioning (Q&P) steels have emerged as highly promising contenders for automotive applications due to their exceptional blend of high strength and ductility, achieved through transformation-induced plasticity associated with retained austenite (RA). Hence, ensuring precise tailoring of RA content and morphology is crucial for Q&P steels. The present investigation aims to study the effect of quenching and partitioning times on RA stability, and the mechanical properties of 0.26C-1.87Mn-0.99Al-0.45Si steel subjected to hot rolling followed by direct quenching and partitioning (DQP). This present research introduces a new microstructural-based approach for identifying the optimal quenching and partitioning times to achieve a microstructure comprising of thin films of inter-lath austenite between martensite laths. DQP steels with longer quenching time exhibit blocky RA islands of smaller sizes. On the other hand, with a shorter quenching time, the microstructure contains a larger fraction of RA with higher carbon content, and this RA is predominantly film type along with small-sized blocky RA islands. This results in an excellent combination of mechanical properties (UTS of 1250 ± 39 MPa and % elongation to failure of 16%). The post-tensile microstructures were also examined using transmission electron microscopy, and film-type RA appears more resistant to strain-induced transformation.

{"title":"Influence of Quenching and Partitioning Times on Austenite Stability and Tensile Properties of CMnAlSi Quenching and Partitioning Steel","authors":"Chintada Umasankar,&nbsp;Apoorv Sobti,&nbsp;S. Sankaran,&nbsp;Uday Chakkingal","doi":"10.1007/s11665-024-10310-2","DOIUrl":"10.1007/s11665-024-10310-2","url":null,"abstract":"<div><p>Quenching and partitioning (Q&amp;P) steels have emerged as highly promising contenders for automotive applications due to their exceptional blend of high strength and ductility, achieved through transformation-induced plasticity associated with retained austenite (RA). Hence, ensuring precise tailoring of RA content and morphology is crucial for Q&amp;P steels. The present investigation aims to study the effect of quenching and partitioning times on RA stability, and the mechanical properties of 0.26C-1.87Mn-0.99Al-0.45Si steel subjected to hot rolling followed by direct quenching and partitioning (DQP). This present research introduces a new microstructural-based approach for identifying the optimal quenching and partitioning times to achieve a microstructure comprising of thin films of inter-lath austenite between martensite laths. DQP steels with longer quenching time exhibit blocky RA islands of smaller sizes. On the other hand, with a shorter quenching time, the microstructure contains a larger fraction of RA with higher carbon content, and this RA is predominantly film type along with small-sized blocky RA islands. This results in an excellent combination of mechanical properties (UTS of 1250 ± 39 MPa and % elongation to failure of 16%). The post-tensile microstructures were also examined using transmission electron microscopy, and film-type RA appears more resistant to strain-induced transformation.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 23","pages":"13311 - 13326"},"PeriodicalIF":2.2,"publicationDate":"2024-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142789228","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Air Oxidation Behavior of Sanicro-25 with Different Surface Finishes 不同表面处理的 Sanicro-25 在空气中的氧化行为
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-16 DOI: 10.1007/s11665-024-10042-3
Ch. Jagadeeswara Rao, M. Aishwarya, Avinash Kumar, P. Thilagavathy, S. Ningshen

Sanicro-25 is a high-temperature material used as the structural material for steam superheaters and reheaters in advanced ultra-supercritical power plants. The air oxidation behavior of Sanicro-25 with various surface roughnesses is being assessed at 650 °C for about 1000 h. Different surface-roughened samples were studied, namely polishing the sample up to diamond finish, grinding up to (80-grit finish and 600-grit finish) and grit blasted. The diamond finish sample showed more weight gain than others, and higher weight gain was observed in the initial oxidation stage. Attributed to different surface preparations leads to defects at different levels, which further alters the diffusion of various elements. The diamond finish sample showed the presence of Cr-rich oxides, and other samples showed the presence of Fe-rich oxides. Smooth surfaces promoted the formation of thick protective oxide scales.

Sanicro-25 是一种高温材料,在先进的超超临界发电厂中用作蒸汽过热器和再热器的结构材料。研究了不同表面粗化样品,即抛光至金刚石表面、研磨至(80 级表面和 600 级表面)和喷砂。与其他样品相比,金刚石表面处理样品的重量增加更多,而且在初始氧化阶段观察到的重量增加也更多。不同的表面处理工艺会导致不同程度的缺陷,从而进一步改变各种元素的扩散。金刚石表面处理样品显示存在富含铬的氧化物,而其他样品则显示存在富含铁的氧化物。光滑的表面促进了厚厚的保护性氧化物鳞片的形成。
{"title":"Air Oxidation Behavior of Sanicro-25 with Different Surface Finishes","authors":"Ch. Jagadeeswara Rao,&nbsp;M. Aishwarya,&nbsp;Avinash Kumar,&nbsp;P. Thilagavathy,&nbsp;S. Ningshen","doi":"10.1007/s11665-024-10042-3","DOIUrl":"10.1007/s11665-024-10042-3","url":null,"abstract":"<div><p>Sanicro-25 is a high-temperature material used as the structural material for steam superheaters and reheaters in advanced ultra-supercritical power plants. The air oxidation behavior of Sanicro-25 with various surface roughnesses is being assessed at 650 °C for about 1000 h. Different surface-roughened samples were studied, namely polishing the sample up to diamond finish, grinding up to (80-grit finish and 600-grit finish) and grit blasted. The diamond finish sample showed more weight gain than others, and higher weight gain was observed in the initial oxidation stage. Attributed to different surface preparations leads to defects at different levels, which further alters the diffusion of various elements. The diamond finish sample showed the presence of Cr-rich oxides, and other samples showed the presence of Fe-rich oxides. Smooth surfaces promoted the formation of thick protective oxide scales.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 24","pages":"13882 - 13896"},"PeriodicalIF":2.2,"publicationDate":"2024-10-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s11665-024-10042-3.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142826392","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Analysis of the Mechanical Characteristics and Properties of a Carbon Fiber–Nylon Composite Influence of the Factors of the Fused Deposition Modeling
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-10-14 DOI: 10.1007/s11665-024-10150-0
Ashok Kumar Palaniappan, Ravi Kumar Krishnan, Pradeep Vasanaperumal, Karthikeyan Rajendiran

Experiments using carbon fiber reinforcing nylon composite produced by fused deposition modeling were conducted to determine mechanical parameters such as impact strength, tensile strength, and flexural strength. Four parameters—layer thickness, printing speed, raster angle, infill density, and twenty-seven runs—were used in the Box–Behnken technique of experimental design. Carbon fiber–nylon composite materials have flexural strengths that range from 20.12 to 25.89 N/mm2, tensile strengths that range from 22.75 to 34.35 N/mm2, and impact strengths that range from 0.37 to 0.72 kJ/m2. Tensile strength was significantly affected by printing speed, while impact and flexural strength was mainly influenced by layer thickness and raster angle. A scanning electron microscope was used on the broken sample to investigate the failure mechanism. Cavities, hillocks, smearing, fracture, ridges, pores, clusters, particle pullout, delamination, deep hole, protrusion, void, crack, infill gap, and interface all have an impact on composite fracture mechanisms.

{"title":"Analysis of the Mechanical Characteristics and Properties of a Carbon Fiber–Nylon Composite Influence of the Factors of the Fused Deposition Modeling","authors":"Ashok Kumar Palaniappan,&nbsp;Ravi Kumar Krishnan,&nbsp;Pradeep Vasanaperumal,&nbsp;Karthikeyan Rajendiran","doi":"10.1007/s11665-024-10150-0","DOIUrl":"10.1007/s11665-024-10150-0","url":null,"abstract":"<div><p>Experiments using carbon fiber reinforcing nylon composite produced by fused deposition modeling were conducted to determine mechanical parameters such as impact strength, tensile strength, and flexural strength. Four parameters—layer thickness, printing speed, raster angle, infill density, and twenty-seven runs—were used in the Box–Behnken technique of experimental design. Carbon fiber–nylon composite materials have flexural strengths that range from 20.12 to 25.89 N/mm<sup>2</sup>, tensile strengths that range from 22.75 to 34.35 N/mm<sup>2</sup>, and impact strengths that range from 0.37 to 0.72 kJ/m<sup>2</sup>. Tensile strength was significantly affected by printing speed, while impact and flexural strength was mainly influenced by layer thickness and raster angle. A scanning electron microscope was used on the broken sample to investigate the failure mechanism. Cavities, hillocks, smearing, fracture, ridges, pores, clusters, particle pullout, delamination, deep hole, protrusion, void, crack, infill gap, and interface all have an impact on composite fracture mechanisms.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 23","pages":"12976 - 12989"},"PeriodicalIF":2.2,"publicationDate":"2024-10-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142789385","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Journal of Materials Engineering and Performance
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