Micro-shear Bond Strength of Self-Adhesive Versus Conventional Low-viscosity Composite Resins: In vitro Study

Cassia Thaís Iurkiv Zanatta, Poliana Maria de Faveri Cardoso, Veridiana Camilotti, M. J. Mendonça, Júlio Katuhide Ueda
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Abstract

Aims: This study aimed to evaluate the micro-shear bond strength of a self-adhesive versus conventional low-viscosity composite resins adhered to enamel. Study Design: In vitro study. Place and Duration of Study: Dental Clinic of the Western State University of Paraná, between October 2022 and September 2023. Methodology: In this in vitro study, the crowns of ten bovine incisor teeth were separated from the roots and embedded in polyvinyl chloride cylinders with acrylic resin. The teeth were divided into two groups (n=5) according to the type of low-viscosity composite resin used on the enamel, resulting in a total of fifteen specimens: one group with self-adhesive composite resin and another with conventional composite resin. Specimens measuring 3 × 2 mm were prepared with low-viscosity composite resin and applied to the adhesive areas according to their respective groups. The micro-shear test was carried out after 7 days of immersion in distilled water in a universal mechanical testing machine with a 50 kg load cell. The statistical analysis in this study employed the Shapiro-Wilk test to assess data normality. Due to non-normal distribution, the non-parametric Mann-Whitney U test was utilized for group comparisons (p < 0.001). Supplementary analyses were performed using the Dwass-Steel-Critchlow-Fligner (DSCF) test for multiple comparisons (p < 0.001) to detect intergroup differences. Fractures were analyzed using a stereoscopic magnifying glass at 40x magnification. Results: The lowest micro-shear bond strength was observed in the self-adhesive composite resin group, while the highest was observed in the conventional composite resin group. On average, the micro-shear bond strength was higher for the conventional composite resin group compared to the self-adhesive composite resin group (p < 0.001). Most fractures in the conventional composite resin group were mixed, whereas in the Self-Adhesive composite resin group they were predominantly adhesive. Conclusion: Based on this study, it can be concluded that self-adhesive flowable composite resin exhibited lower enamel bond strength values compared to conventional flowable composite resin.
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自粘性与传统低粘度复合树脂的微剪切粘接强度:体外研究
研究目的:本研究旨在评估自粘树脂与传统低粘度复合树脂粘附在牙釉质上的微剪切粘接强度。研究设计:体外研究。研究地点和时间:巴拉那西部州立大学牙科诊所,2022 年 10 月至 2023 年 9 月。研究方法在这项体外研究中,将 10 颗牛门牙的牙冠与牙根分离,并用丙烯酸树脂将其嵌入聚氯乙烯圆柱体中。根据在牙釉质上使用的低粘度复合树脂类型,将这些牙齿分为两组(n=5),共有 15 个试样:一组使用自粘复合树脂,另一组使用传统复合树脂。用低粘度复合树脂制备了 3 × 2 毫米的试样,并按照各自的组别涂抹在粘合区域。在蒸馏水中浸泡 7 天后,在带有 50 千克载荷传感器的通用机械试验机中进行微剪切试验。本研究的统计分析采用 Shapiro-Wilk 检验来评估数据的正态性。由于非正态分布,在进行组间比较时采用了非参数曼-惠特尼 U 检验(P < 0.001)。补充分析采用 Dwass-Steel-Critchlow-Fligner (DSCF) 检验进行多重比较(P < 0.001),以检测组间差异。使用放大 40 倍的立体放大镜分析骨折情况。结果自粘复合树脂组的微剪切粘接强度最低,而传统复合树脂组最高。平均而言,传统复合树脂组的微剪切粘接强度高于自粘复合树脂组(p < 0.001)。传统复合树脂组的大多数裂缝是混合性的,而自粘复合树脂组的裂缝主要是粘接性的。结论根据这项研究可以得出结论,与传统的可流动复合树脂相比,自粘性可流动复合树脂的牙釉质粘结强度值较低。
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