On the Effect of the Melt Cooling Rate upon Spinning on the Structure of the Surface Layers of Fe77Ni1Si9B13 Alloy Ribbons

IF 0.8 4区 物理与天体物理 Q4 PHYSICS, APPLIED Technical Physics Letters Pub Date : 2024-03-28 DOI:10.1134/s1063785024700184
V. I. Lad’yanov, M. S. Konovalov, M. I. Mokrushina, A. I. Shilyaev, D. P. Ardasheva
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Abstract

Fast-quenched ribbons with thicknesses of 200, 50, 30, and 20 μm have been obtained by melt spinning at hardening disk rotation speeds of 500, 1500, 2500, and 3500 rpm, respectively. The chemical composition of the ribbons has been determined by atomic emission spectroscopy on a Spectroflame Modula S spectrometer. X-ray diffraction patterns of the ribbons have obtained on a DRON-6 diffractometer (CuKα radiation) with a graphite monochromator. The effect of the melt cooling rate on the structural state of the contact and free sides of the Fe77Ni1Si9B13 alloy ribbons has been examined. It has been established that, by increasing the melt cooling rate, one can obtain fast-quenched Fe77Ni1Si9B13 alloy ribbons with different structures: X-ray amorphous at 3500, 2500, and 1500 rpm and crystalline at 500 rpm. Cooling of the melt at a quenching disk rotation speed of 500 rpm makes it possible to obtain Fe77Ni1Si9B13 alloy ribbons with crystallographic structures of three types: A2, C16, and D03 (A2 corresponds to the α-Fe(Si) phase; C16, to the Fe2B phase; and D03, to the Fe3Si phase). In the surface layers on the ribbon free side, texturing of the Fe3Si phase has been detected. It is noted that the crystal structure of the ribbons obtained by melt cooling on a quenching disk at a rotation speed of 500 rpm differs from the structure of the ribbons of this alloy crystallized from the amorphous state by annealing.

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纺丝时熔体冷却速率对 Fe77Ni1Si9B13 合金带表面层结构的影响
摘要通过在硬化盘转速分别为 500、1500、2500 和 3500 rpm 的条件下进行熔融纺丝,获得了厚度分别为 200、50、30 和 20 μm 的快速淬火带。色带的化学成分是通过 Spectroflame Modula S 光谱仪上的原子发射光谱测定的。色带的 X 射线衍射图样是在带有石墨单色器的 DRON-6 衍射仪(CuKα 辐射)上获得的。研究了熔体冷却速度对 Fe77Ni1Si9B13 合金带接触面和自由面结构状态的影响。结果表明,通过提高熔体冷却速度,可以获得具有不同结构的快速淬火 Fe77Ni1Si9B13 合金带:在 3500、2500 和 1500 转/分钟时为 X 射线无定形带,在 500 转/分钟时为结晶带。以 500 转/分的淬火盘转速冷却熔体,可获得具有三种结晶结构的 Fe77Ni1Si9B13 合金带:A2、C16 和 D03(A2 相当于 α-Fe(Si)相;C16 相当于 Fe2B 相;D03 相当于 Fe3Si 相)。在无色带一侧的表层中,检测到了 Fe3Si 相的纹理。值得注意的是,在转速为 500 转/分的淬火盘上熔融冷却得到的带状材料的晶体结构与通过退火从无定形状态结晶出来的带状材料的晶体结构不同。
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来源期刊
Technical Physics Letters
Technical Physics Letters 物理-物理:应用
CiteScore
1.50
自引率
0.00%
发文量
44
审稿时长
2-4 weeks
期刊介绍: Technical Physics Letters is a companion journal to Technical Physics and offers rapid publication of developments in theoretical and experimental physics with potential technological applications. Recent emphasis has included many papers on gas lasers and on lasing in semiconductors, as well as many reports on high Tc superconductivity. The excellent coverage of plasma physics seen in the parent journal, Technical Physics, is also present here with quick communication of developments in theoretical and experimental work in all fields with probable technical applications. Topics covered are basic and applied physics; plasma physics; solid state physics; physical electronics; accelerators; microwave electron devices; holography.
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