Ranveig Flatabø , Sabrina D. Eder , Thomas Reisinger , Gianangelo Bracco , Peter Baltzer , Björn Samelin , Bodil Holst
{"title":"Reflection imaging with a helium zone plate microscope","authors":"Ranveig Flatabø , Sabrina D. Eder , Thomas Reisinger , Gianangelo Bracco , Peter Baltzer , Björn Samelin , Bodil Holst","doi":"10.1016/j.ultramic.2024.113961","DOIUrl":null,"url":null,"abstract":"<div><p>Neutral helium atom microscopy is a novel microscopy technique which offers strictly surface-sensitive, non-destructive imaging. Several experiments have been published in recent years where images are obtained by scanning a helium beam spot across a surface and recording the variation in scattered intensity at a fixed total scattering angle <span><math><msub><mrow><mi>θ</mi></mrow><mrow><mi>S</mi><mi>D</mi></mrow></msub></math></span> and fixed incident angle <span><math><msub><mrow><mi>θ</mi></mrow><mrow><mi>i</mi></mrow></msub></math></span> relative to the overall surface normal. These experiments used a spot obtained by collimating the beam (referred to as helium pinhole microscopy). Alternatively, a beam spot can be created by focusing the beam with an atom optical element. However up till now imaging with a focused helium beam has only been demonstrated in transmission (using a zone plate). Here we present the first reflection images obtained with a focused helium beam (also using a zone plate). Images are obtained with a spot size (FWHM) down to <span><math><mrow><mn>4</mn><mo>.</mo><mn>7</mn><mspace></mspace><mi>μ</mi><mi>m</mi></mrow></math></span> <span><math><mrow><mo>±</mo><mn>0</mn><mo>.</mo><mn>5</mn><mspace></mspace><mi>μ</mi></mrow></math></span>m, and we demonstrate focusing down to a spot size of about <span><math><mrow><mn>1</mn><mspace></mspace><mi>μ</mi><mi>m</mi></mrow></math></span>. Furthermore, we present experiments measuring the scattering distribution from a focused helium beam spot. The experiments are done by varying the incoming beam angle <span><math><msub><mrow><mi>θ</mi></mrow><mrow><mi>i</mi></mrow></msub></math></span> while keeping the beam-detector angle <span><math><msub><mrow><mi>θ</mi></mrow><mrow><mi>S</mi><mi>D</mi></mrow></msub></math></span> and the point where the beam spot hits the surface fixed - in essence, a microscopy scale realization of a standard helium atom scattering experiment. Our experiments are done using an electron bombardment detector with adjustable signal accumulation, developed particularly for helium microscopy.</p></div>","PeriodicalId":23439,"journal":{"name":"Ultramicroscopy","volume":"261 ","pages":"Article 113961"},"PeriodicalIF":2.1000,"publicationDate":"2024-03-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S0304399124000408/pdfft?md5=ec4696109d63195bfa1b2266f49757f6&pid=1-s2.0-S0304399124000408-main.pdf","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Ultramicroscopy","FirstCategoryId":"5","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0304399124000408","RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"MICROSCOPY","Score":null,"Total":0}
引用次数: 0
Abstract
Neutral helium atom microscopy is a novel microscopy technique which offers strictly surface-sensitive, non-destructive imaging. Several experiments have been published in recent years where images are obtained by scanning a helium beam spot across a surface and recording the variation in scattered intensity at a fixed total scattering angle and fixed incident angle relative to the overall surface normal. These experiments used a spot obtained by collimating the beam (referred to as helium pinhole microscopy). Alternatively, a beam spot can be created by focusing the beam with an atom optical element. However up till now imaging with a focused helium beam has only been demonstrated in transmission (using a zone plate). Here we present the first reflection images obtained with a focused helium beam (also using a zone plate). Images are obtained with a spot size (FWHM) down to m, and we demonstrate focusing down to a spot size of about . Furthermore, we present experiments measuring the scattering distribution from a focused helium beam spot. The experiments are done by varying the incoming beam angle while keeping the beam-detector angle and the point where the beam spot hits the surface fixed - in essence, a microscopy scale realization of a standard helium atom scattering experiment. Our experiments are done using an electron bombardment detector with adjustable signal accumulation, developed particularly for helium microscopy.
期刊介绍:
Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.