Impact of Assorted Temperature on Yield and Surface Morphology of Multiple Layers of Carbon Nanotubes by Spurt Pyrolysis Techniques

N. M. Kumar, S. Paulsingarayar, S. Nagaraja, S. Kalaiselvan
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Abstract

Nanoscale carbon tubes (also referred as CNTs) along with other nanostructures made from carbon could keep you amused as you waiting for your chance to participate in this nanotechnology. Research on carbon nanotubes has attracted an enormous amount of focus from researchers across the world for the significant function that it could have in the growing field of nanotechnology. The MLCNTs were made using these temperatures as the operational parameters using a fatty acid methyl ester formed from peanut oil as a precursor at a flow rate of 20 mL per hour in an environment comprised of argon. The intention of this research is to examine a usual green originator for the production of multiple layer carbon nanotubes (MLCNTs) using the methyl ester of a fatty acid of peanut oil at temperature that range from 725°C to 875°C with intervals of 75°C on Fe-Co assisted on Silica within an atmosphere of argon. The investigation will be concentrated on the production of MLCNTs on Fe-Co assisted on Silica. The as-grown carbon nanomaterials have been studied using SEM, HRTEM, XRD, and Raman spectroscopic research. We observed that the yield and diameter of the as-grown MLCNTs were not the same across the entire board for temperatures. The crystalline temperature of the CNTs climbed from 725 degrees Celsius to 800 degrees Celsius initially, and eventually it dropped from 800 degrees Celsius to 875 degrees Celsius. The temperature at which MLCNTs are created may have a bearing on the level of graphitization that they'll show.
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喷射热解技术中各种温度对多层碳纳米管产量和表面形态的影响
纳米级碳管(也称 CNT)以及其他由碳制成的纳米结构可以让您在等待机会参与这项纳米技术的过程中乐此不疲。对碳纳米管的研究吸引了全世界研究人员的大量关注,因为它在不断发展的纳米技术领域中具有重要作用。在氩气环境中,使用花生油中的脂肪酸甲酯作为前体,以每小时 20 毫升的流速,以上述温度作为操作参数,制造出了 MLCNT。本研究的目的是在氩气环境中,使用花生油脂肪酸甲酯,在 725°C 至 875°C 的温度范围内,以 75°C 的间隔,在二氧化硅上的铁-钴辅助下,研究生产多层碳纳米管 (MLCNT) 的常用绿色原丝。研究将集中于在二氧化硅上的 Fe-Co 辅助材料上生产 MLCNT。我们使用 SEM、HRTEM、XRD 和拉曼光谱研究了已生长的碳纳米材料。我们观察到,在不同温度下生长的 MLCNT 的产量和直径并不相同。碳纳米管的结晶温度最初从 725 摄氏度上升到 800 摄氏度,最后又从 800 摄氏度下降到 875 摄氏度。制造 MLCNT 的温度可能会影响它们的石墨化程度。
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