Synthesis and Characterization of Ni/Al Layered Double Hydroxides Composite Based-Material with Chitosan, Cellulose, and Graphene Oxide

Amri Amri, Zaqiya Artha Zahara, P. M. S. B. Siregar, Zulkarnain Zulkarnain, A. Wijaya
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Abstract

In this study, the synthesis of composite materials produced from Ni/Al with three types of carbon-based materials namely chitosan (Ch), cellulose (Ce), and graphene oxide (GO) was successfully carried out supported by X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR), and Brunauer-Emmett-Teller (BET) analysis. The combined characteristics of the two starting materials are present in the composite material based on XRD and FT-IR data. The surface area of Ni/Al-LDH increased after compositing with Ch, Ce, and GO, from 3.3 m2/g to 9.5 m2/g in Ni/Al-Ch, 5.1 m2/g in Ni/Al-Ce, and 78.4 m2/g in Ni/Al-GO. These findings indicate that the materials are suitable for various applications such as photocatalytic and adsorption as effective materials in further research.
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基于壳聚糖、纤维素和氧化石墨烯的镍/铝层状双氢氧化物复合材料的合成与表征
在本研究中,通过 X 射线衍射 (XRD)、傅立叶变换红外光谱 (FT-IR) 和布鲁瑙尔-艾美特-泰勒 (BET) 分析,成功合成了镍/铝与三种碳基材料(即壳聚糖 (Ch)、纤维素 (Ce) 和氧化石墨烯 (GO))的复合材料。根据 XRD 和傅立叶变换红外光谱数据,复合材料中存在两种起始材料的综合特性。与 Ch、Ce 和 GO 复合后,Ni/Al-LDH 的表面积增加了,Ni/Al-Ch 从 3.3 m2/g 增加到 9.5 m2/g,Ni/Al-Ce 为 5.1 m2/g,Ni/Al-GO 为 78.4 m2/g。这些研究结果表明,这些材料适用于各种应用,如光催化和吸附,是有待进一步研究的有效材料。
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