Effect of Mercerization on the Crystallographic, Macromolecular, and Thermal Properties of Plantain Fibers for Fiber Reinforced Composite

Patrick Ehi Imoisili, Tien Chien Jen
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Abstract

In this research, natural fibers (NF) were obtained from plantain pseudo stem. The extracted plantain fibers (PF) were modified by mercerization under diverse conditions in terms of treatment time and concentration. The crystallographic structures and macromolecular properties, and surface extracted PF were all influenced by the modification process. Improvements in thermal properties were observed along with increases in the crystallite size, and degree of crystallinity as revealed by x-ray diffraction (XRD) analysis. FTIR spectroscopy confirmed partial removal of wax, lignin, and hemicellulose. Bulk density was also observed to change under treatment conditions, while Scanning electron microscope (SEM) imagery demonstrates how the treatment altered the surface of the PF. A considerable change in the macromolecular and structural characteristics of plantain fiber was observed under optimum treatment conditions.
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丝光处理对用于纤维增强复合材料的车前草纤维的晶体学、大分子和热性能的影响
本研究从车前草假茎中提取天然纤维(NF)。在不同的处理时间和浓度条件下,对提取的车前草纤维(PF)进行丝光改性。改性过程对提取的车前草纤维(PF)的晶体结构、大分子特性和表面均产生了影响。X 射线衍射(XRD)分析表明,随着晶粒尺寸和结晶度的增加,热性能也得到了改善。傅立叶变换红外光谱证实了蜡质、木质素和半纤维素的部分去除。在处理条件下,还观察到体积密度发生了变化,而扫描电子显微镜(SEM)图像则显示了处理如何改变了聚对苯二甲酸乙二醇酯的表面。在最佳处理条件下,车前草纤维的大分子和结构特征发生了显著变化。
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