Tribological characterization of SAE20W40 lubricant added with surface activated nanoparticles (Al2O3 and SiO2)

S. Ramprakaash, K. Muralidharan, R. Vaira Vignesh, R. Senthil Kumar, M. Govindaraju, A. Baghad
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Abstract

This research work focuses on the performance characteristics of the standard SAE20W40 lubricant with the addition of nanoparticles (aluminum oxide (Al2O3) and silicon dioxide (SiO2) in equal proportion). The nanoparticles were surface-activated using oleic acid to homogenize the lubricant dispersion. The lubricant was added with 0.1, 0.3, and 0.5 wt% of nanoparticles and subjected to a mechano-thermal process to synthesize nanolubricant. The physio-chemical properties (flash point, fire point, thermal stability, kinematic viscosity, acid value, and iodine value) and tribological characteristics (specific wear rate, friction coefficient, and wear mechanism) of the nanolubricant were determined and correlated with dispersed nanoparticles. Instrumental characterization of SEM, EDS, TEM, FT-IR, and UV-Vis tests were performed to validate the surface-activated nanolubricant. The base lubricant demonstrated favorable tribological characteristics when enhanced with 0.1 wt% additives.
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添加了表面活性纳米颗粒(Al2O3 和 SiO2)的 SAE20W40 润滑油的摩擦学特性分析
这项研究工作的重点是在标准 SAE20W40 润滑油中添加纳米颗粒(氧化铝 (Al2O3) 和二氧化硅 (SiO2) 的比例相同)后的性能特性。使用油酸对纳米颗粒进行表面活性处理,使润滑油分散体均匀化。在润滑剂中分别添加 0.1、0.3 和 0.5 wt% 的纳米粒子,并通过机械热处理合成纳米润滑剂。测定了纳米润滑剂的物理化学特性(闪点、燃点、热稳定性、运动粘度、酸值和碘值)和摩擦学特性(比磨损率、摩擦系数和磨损机理),并将其与分散的纳米粒子联系起来。为了验证表面活性纳米润滑剂,还进行了扫描电镜、电子显微镜、透射电镜、傅立叶变换红外光谱和紫外可见光测试等仪器表征。当添加 0.1 wt% 的添加剂后,基础润滑剂表现出了良好的摩擦学特性。
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