Characterization of Composite Films from Taro Starch Modified with the Addition of Duck Bone Gelatin

Trias Ayu Ayu Laksanawati, M. H. Khirzin, Maghfirotul Amaniyah, Karina Meidayanti
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Abstract

In this study, composite films were prepared from modified taro starch with the addition of duck bone gelatin using varying percentages (0%, 5%, 15%, 25%, 35% of the total solids weight) by solution casting method. The mixing of duck bone gelatin on taro starch films was studied as a new approach for composite films from natural materials that are environmentally friendly and have good physical properties. This study aimed to obtain information on the effect of the percentage variation of duck bone gelatin on the composite film on the density, transparency, crystallinity and thermal properties. The results of revealed that the addition of duck bone gelatin concentration had no significant effect (p>0.05) on the density of the composite films, but had a significant effect (p<0.05) on the transparency and termal properties. Crystallinity analysis using X-ray diffraction (XRD) technique showed that the composite films product has a semicrystalline structure with low crystallinity. DSC scan showed that the composite film with the addition of 5% duck bone gelatin gave high thermal stability values ​​with melting temperature (Tm) 181.86°C and melting enthalpy (ΔHm) 252.73 J/g. The TGA results confirmed that the thermal stability of the composite film at the concentration of 5% duck bone gelatin had a weight loss of 37.48 % in the temperature range (296.74-500°C).
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添加了鸭骨明胶的芋头淀粉改性复合薄膜的表征
本研究采用溶液浇铸法,在改性芋头淀粉中添加不同比例(占总固体重量的 0%、5%、15%、25%、35%)的鸭骨明胶,制备了复合薄膜。鸭骨明胶在芋头淀粉薄膜上的混合研究是利用天然材料制作复合薄膜的一种新方法,既环保又具有良好的物理性能。这项研究旨在了解鸭骨明胶在复合薄膜中的比例变化对密度、透明度、结晶度和热性能的影响。研究结果表明,鸭骨明胶浓度的增加对复合薄膜的密度没有显著影响(p>0.05),但对透明度和热性能有显著影响(p<0.05)。利用 X 射线衍射(XRD)技术进行的结晶度分析表明,复合薄膜产品具有半晶体结构,结晶度较低。DSC 扫描显示,添加 5% 鸭骨明胶的复合薄膜具有较高的热稳定性,熔化温度(Tm)为 181.86°C,熔化焓(ΔHm)为 252.73 J/g。热重分析结果证实,添加 5%鸭骨明胶的复合薄膜的热稳定性在温度范围(296.74-500°C)内的失重率为 37.48%。
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