Experimental analysis of blended nanocomposites processed using compression molded microwave process

Gaurav Arora
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Abstract

Microwave irradiation has emerged as a versatile and efficient method for synthesizing polymer nanocomposites, offering advantages such as selectivity, speed, and effectiveness in heating materials. This study explores the blending of low-density polyethylene (LDPE) and polypropylene (PP) with carbon nanotubes (CNTs) using microwave processing. The nanocomposites were characterized for their mechanical properties through tensile and fracture toughness tests. Results indicate that LDPE/CNT blended with PP/CNT pellets exhibited improved Young’s modulus and fracture toughness, while LDPE/CNT blended with PP/CNT powder showed enhanced stiffness and fracture toughness. The critical stress intensity factor ( KIC) increased with higher proportions of PP in both cases, signifying improved crack resistance. XRD and SEM analyses confirmed enhanced crystallinity and proper bonding between polymers and CNTs. Overall, this study demonstrates the potential of microwave processing in producing nanocomposites with enhanced mechanical properties, offering a promising avenue for engineering applications.
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使用压缩成型微波工艺加工的混合纳米复合材料的实验分析
微波辐照是合成聚合物纳米复合材料的一种多功能高效方法,具有选择性强、速度快、加热材料效果好等优点。本研究探讨了利用微波处理将低密度聚乙烯(LDPE)和聚丙烯(PP)与碳纳米管(CNT)共混的方法。通过拉伸和断裂韧性测试对纳米复合材料的机械性能进行了表征。结果表明,与 PP/CNT 颗粒混合的 LDPE/CNT 具有更高的杨氏模量和断裂韧性,而与 PP/CNT 粉末混合的 LDPE/CNT 则具有更高的刚度和断裂韧性。在这两种情况下,临界应力强度因子(KIC)都随着 PP 比例的增加而提高,这表明抗裂性得到了改善。XRD 和 SEM 分析证实了聚合物和 CNT 之间结晶度的提高和适当的结合。总之,这项研究证明了微波加工在生产具有更强机械性能的纳米复合材料方面的潜力,为工程应用提供了一条前景广阔的途径。
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