Analysis of the State of the Surface Layer of the SAP-2 Composite Alloy after Irradiation with a High-Power Ion Beam

T. V. Panova, V. S. Kovivchak
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Abstract

The effect of a high-power ion beam of nanosecond duration on the phase composition and morphology of the surface of aluminum composite material SAP-2 is studied. It is found that after irradiation with a high-power ion beam under all irradiation modes used in the experiments no changes in the phase composition are observed. However, the observed shifts and broadening of the diffraction peaks from irradiated samples indicate the formation of residual stresses and transformation of the initial dislocation structure. The observed decrease in the dislocation density results in a decrease in the microhardness of SAP-2 irradiated at current densities of 50 and 100 A/cm2. It is shown that the increase in the ion-current density leads to an increase in the oxygen fraction in the surface layer of SAP-2, which is apparently associated with the partial evaporation of aluminum and an increase in the concentration of inclusions of Al2O3, which is part of the material. A nonlinear character of the dependence of the average ratio of the oxygen content to aluminum on the ion-current density of the beam is observed, the maximum value of which is recorded upon irradiation with a beam-current density of 100 A/cm2. Intense heating of the SAP-2 surface under ion-beam irradiation leads to changes in the dispersion of Al2O3 inclusions on the irradiated surface. The maximum coagulation of Al2O3 particles is found in the case of irradiation by a high-power ion beam with a current density of 100 A/cm2.

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高能离子束辐照后 SAP-2 复合材料表层状态分析
摘要 研究了纳秒级大功率离子束对铝复合材料 SAP-2 表面相组成和形态的影响。研究发现,在实验中使用的所有辐照模式下,经过大功率离子束辐照后,相组成均未发生变化。然而,从辐照样品中观察到的衍射峰的移动和变宽表明了残余应力的形成和初始位错结构的转变。在电流密度为 50 和 100 A/cm2 时,观察到的位错密度下降导致辐照 SAP-2 的显微硬度下降。研究表明,离子电流密度的增加会导致 SAP-2 表层的氧含量增加,这显然与铝的部分蒸发和材料中 Al2O3 杂质浓度的增加有关。氧含量与铝含量的平均比值与离子束的离子电流密度呈非线性关系,当离子束电流密度为 100 A/cm2 时,氧含量与铝含量的平均比值达到最大值。在离子束辐照下,SAP-2 表面的强烈加热导致辐照表面上 Al2O3 包裹体的分散发生变化。在电流密度为 100 A/cm2 的大功率离子束辐照下,Al2O3 粒子的凝结程度最大。
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来源期刊
CiteScore
0.90
自引率
25.00%
发文量
144
审稿时长
3-8 weeks
期刊介绍: Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.
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