Recovery of residual polyamide (PA12) from polymer powder bed fusion additive manufacturing process through a binder jetting process

IF 3.4 4区 工程技术 Q1 ENGINEERING, MECHANICAL Rapid Prototyping Journal Pub Date : 2024-05-03 DOI:10.1108/rpj-05-2023-0177
Cesar O. Balderrama-Armendáriz, Sergio Esteban Arbelaez-Rios, Santos-Adriana Martel-Estrada, A. Maldonado-Macías, Eric MacDonald, J. Aguilar-Duque
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Abstract

Purpose This study aims to propose the reuse of PA12 (powder) in another AM process, binder jettiinng, which is less sensitive to the chemical and mechanical degradation of the powder after multiple cycles in the laser system. Design/methodology/approach The experimental process for evaluating the reuse of SLS powders in a subsequent binder jetting process consists of four phases: powder characterization, bonding analysis, mixture testing and mixture characteristics. Analyses were carried out using techniques such as Fourier Transform Infrared Spectroscopy, scanning electron microscopy, thermogravimetric analysis and stress–strain tests for tension and compression. The surface roughness, color, hardness and density of the new mixture were also determined to find physical characteristics. A Taguchi design L8 was used to search for a mixture with the best mechanical strength. Findings The results indicated that the integration of waste powder PA12 with calcium sulfate hemihydrate (CSH) generates appropriate particle distribution with rounded particles of PA12 that improve powder flowability. The micropores observed with less than 60 µm, facilitated binder and infiltrant penetration on 3D parts. The 60/40 (CSH-PA12) mixture with epoxy resin postprocessing was found to be the best-bonded mixture in mechanical testing, rugosity and hardness results. The new CSH-PA12 mixture resulted lighter and stronger than the CSH powder commonly used in binder jetting technology. Originality/value This study adds value to the polymer powder bed fusion process by using its waste in a circular process. The novel reuse of PA12 waste in an established process was achieved in an accessible and economical manner.
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通过粘合剂喷射工艺从聚合物粉末床熔融增材制造工艺中回收残余聚酰胺(PA12)
本研究旨在提出在另一种 AM 工艺(粘合剂喷射)中重复使用 PA12(粉末),这种工艺对粉末在激光系统中多次循环后的化学和机械降解不太敏感。使用傅立叶变换红外光谱、扫描电子显微镜、热重分析以及拉伸和压缩应力应变测试等技术进行了分析。此外,还测定了新混合物的表面粗糙度、颜色、硬度和密度,以发现其物理特性。研究结果表明,废弃粉末 PA12 与半水硫酸钙(CSH)的混合产生了适当的颗粒分布,PA12 颗粒呈圆形,改善了粉末的流动性。观察到的微孔小于 60 µm,有利于粘合剂和浸润剂在三维部件上的渗透。经环氧树脂后处理的 60/40(CSH-PA12)混合物在机械测试、凹凸度和硬度结果中被认为是粘结性最好的混合物。新的 CSH-PA12 混合物比粘结剂喷射技术中常用的 CSH 粉末更轻、更强。在一个成熟的工艺流程中,以方便和经济的方式实现了 PA12 废料的新颖再利用。
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来源期刊
Rapid Prototyping Journal
Rapid Prototyping Journal 工程技术-材料科学:综合
CiteScore
8.30
自引率
10.30%
发文量
137
审稿时长
4.6 months
期刊介绍: Rapid Prototyping Journal concentrates on development in a manufacturing environment but covers applications in other areas, such as medicine and construction. All papers published in this field are scattered over a wide range of international publications, none of which actually specializes in this particular discipline, this journal is a vital resource for anyone involved in additive manufacturing. It draws together important refereed papers on all aspects of AM from distinguished sources all over the world, to give a truly international perspective on this dynamic and exciting area. -Benchmarking – certification and qualification in AM- Mass customisation in AM- Design for AM- Materials aspects- Reviews of processes/applications- CAD and other software aspects- Enhancement of existing processes- Integration with design process- Management implications- New AM processes- Novel applications of AM parts- AM for tooling- Medical applications- Reverse engineering in relation to AM- Additive & Subtractive hybrid manufacturing- Industrialisation
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