Microstructural evolutions of molybdenum‑rhenium (47.5 wt.%) alloy under room and high temperature compressions

IF 4.8 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2024-05-21 DOI:10.1016/j.matchar.2024.114001
Li Huang , Yichao Yang , Jing Liang , Xiaohui Lin , Xuanqiao Gao , Yanchao Li , Hailong Xu , Jianfeng Li , Wen Zhang
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Abstract

Act as a candidate for heat pipe reactor core, molybdenum‑rhenium (47.5 wt%) alloy possesses excellent mechanical properties at a wide temperature range (from room temperature to recrystallized temperature). Compressions at varied temperatures and strain rates were given to study the microstructural evolutions of Mo-47.5Re alloy. Yield strength is similar in sample compressed at 400 °C with high strain rate (1.67 × 10−1 /s) and the one at room temperature with low strain rate (1.67 × 10−3 /s). However, deformation twins are only observed under room temperature and are absent as temperature rises to 400 °C. Thus. Twinning in MoRe alloy is much sensitive to temperature. The microstructure of Mo-47.5Re alloy is quite stable even compression at 1200 °C. Although sub-grains increasing after 1200 °C compressions, no recrystallization was detected. In addition, microstructural evolutions of Mo-47.5Re are outstandingly dependent on strain rates at 400 °C, while are much less obviously at 800 °C and 1200 °C. No phase changes are detected, which verifies good structural stability in Mo-47.5Re.

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钼-铼(47.5 wt.%)合金在室温和高温压缩条件下的微观结构演变
作为热管反应堆堆芯的候选材料,钼-铼(47.5 wt%)合金在很宽的温度范围内(从室温到再结晶温度)都具有优异的机械性能。为了研究钼-47.5Re 合金的微观结构演变,我们在不同温度和应变率下对其进行了压缩。在 400 ℃、高应变率(1.67 × 10-1 /s)下压缩的样品与在室温、低应变率(1.67 × 10-3 /s)下压缩的样品屈服强度相似。然而,只有在室温下才能观察到变形孪晶,当温度升至 400 ℃ 时,变形孪晶就会消失。因此。MoRe 合金中的孪晶对温度非常敏感。Mo-47.5Re 合金的微观结构即使在 1200 ℃下压缩也相当稳定。虽然亚晶粒在 1200 °C 压缩后有所增加,但未发现再结晶现象。此外,在 400 ℃ 时,Mo-47.5Re 的微观结构演变与应变率的关系非常明显,而在 800 ℃ 和 1200 ℃ 时则不那么明显。没有检测到相变,这证明 Mo-47.5Re 具有良好的结构稳定性。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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