Optimizing the Extraction Efficiency of Flaxseed Gum Using a Response Surface Methodology Approach.

IF 2.3 3区 化学 Q3 CHEMISTRY, ANALYTICAL Journal of Analytical Methods in Chemistry Pub Date : 2024-06-12 eCollection Date: 2024-01-01 DOI:10.1155/2024/5135565
Abdessamad Ettouil, Asmaa Oubihi, Hamada Imtara, Khadija Atfaoui, Ramzi A Mothana, Omar M Noman, Mahmoud Tarayrah, Mohammed Ouhssine
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Abstract

The extraction of gum from natural raw materials is of increasing importance in various industries, including food, pharmaceuticals, and cosmetics, particularly due to their emulsifying properties and potential applications as stabilizers and thickeners. This study presents an insight on the influence of changing parameters like reagents and operating condition on yield and some properties of the flax (Linum usitatissimum L.) seed gum. The extraction conditions were meticulously examined using a full factorial design, highlighting the significant impact of pretreatment, seed preparation, and solvent selection on the extraction yield. A response surface methodology (RSM) was then applied to optimize the water/benzoic acid ratio of the pretreatment step, the ethyl alcohol/water ratio, and the medium pH of the extraction method, resulting in a maximum yield of 14.47%. Furthermore, detailed analyses of the chemical and emulsifying properties of the gum were conducted showing emulsifying capacities over 94%, offering promising application prospects, particularly in the food industry.

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利用响应面方法优化亚麻籽胶的提取效率
从天然原料中提取树胶在食品、药品和化妆品等各行各业中的重要性与日俱增,特别是因为树胶具有乳化特性,可用作稳定剂和增稠剂。本研究深入探讨了改变试剂和操作条件等参数对亚麻(Linum usitatissimum L.)籽胶产量和某些特性的影响。采用全因子设计对提取条件进行了细致的研究,突出了预处理、种子制备和溶剂选择对提取率的重要影响。随后,应用响应面方法(RSM)优化了预处理步骤中的水/苯甲酸比例、乙醇/水比例以及萃取方法的介质 pH 值,最终获得了 14.47% 的最高产率。此外,还对树胶的化学和乳化特性进行了详细分析,结果显示其乳化能力超过 94%,应用前景广阔,尤其是在食品行业。
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来源期刊
Journal of Analytical Methods in Chemistry
Journal of Analytical Methods in Chemistry CHEMISTRY, ANALYTICAL-ENGINEERING, CIVIL
CiteScore
4.80
自引率
3.80%
发文量
79
审稿时长
6-12 weeks
期刊介绍: Journal of Analytical Methods in Chemistry publishes papers reporting methods and instrumentation for chemical analysis, and their application to real-world problems. Articles may be either practical or theoretical. Subject areas include (but are by no means limited to): Separation Spectroscopy Mass spectrometry Chromatography Analytical Sample Preparation Electrochemical analysis Hyphenated techniques Data processing As well as original research, Journal of Analytical Methods in Chemistry also publishes focused review articles that examine the state of the art, identify emerging trends, and suggest future directions for developing fields.
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