Preparation and Application of Black Cumin Seed Oil Emulsion with Enhanced Stability for Antimicrobial Treatment of Cellulosic Fabric

IF 2.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Fibers and Polymers Pub Date : 2024-06-18 DOI:10.1007/s12221-024-00601-9
Md. Imran Hosen, Arnob Dhar Pranta, Md. Mehedi Hasan, Md. Syful Islam, Tarikul Islam, Fatama Tous Zohora, Md.Imranul Islam, M. Mahbubul Bashar, Gajanan Bhat
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Abstract

With the growing concern for health and wellness, many textile mills are witnessing a surge in demand for antimicrobial and anti-viral treatments on fabric. The black cumin seed (BCS) is blessed with various antioxidants and antimicrobial active agents, and can be used to develop antimicrobial fabric. The current study aims to prepare a stable emulsion with BCS oil to apply on casual knitted fabric to investigate its anti-bacterial properties. The homogenous emulsions were prepared with Tween-80 surfactant and applied to the fabric by exhaust method. Thus, the emulsions were stable at various temperatures. The surface functional groups of treated fabric were characterized with FT-IR spectroscopy and the surface morphology was visualized with SEM images to confirm the modification. The FT-IR spectrum of treated fabric guaranteed successful modification, presenting the major surface functional groups in the treated fabric. The SEM images further confirmed this phenomenon as the treated fabric exhibited cemented layer deposition of BCS emulsions. The anti-bacterial activity of treated fabric against Bacillus subtilis microbes was measured using the Kirbey–Bauer method. The result showed that the treated fabric demonstrated anti-bacterial activity against B. subtilis with an inhibition zone of 8 mm. The resistive activity against the target bacteria was found active even after a single wash. This was proven through the optical density test which indicated that the fabric can be used for healthcare PPF securing their antimicrobial and anti-viral properties.

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制备和应用稳定性更强的黑孜然籽油乳液对纤维素织物进行抗菌处理
随着人们对健康和保健的日益关注,许多纺织厂对织物进行抗菌和抗病毒处理的需求激增。黑孜然籽(BCS)富含多种抗氧化剂和抗菌活性剂,可用于开发抗菌织物。本研究旨在制备一种稳定的黑孜然籽油乳液,将其涂在休闲针织物上,研究其抗菌特性。研究人员使用吐温-80 表面活性剂制备了均匀的乳液,并通过排气法将其涂在织物上。因此,乳液在不同温度下都很稳定。用傅立叶变换红外光谱对处理过的织物表面官能团进行表征,并用扫描电镜图像观察其表面形态,以确认改性效果。经处理织物的傅立叶变换红外光谱保证了改性的成功,显示了经处理织物的主要表面官能团。扫描电镜图像进一步证实了这一现象,因为处理过的织物呈现出 BCS 乳液的胶结层沉积。使用 Kirbey-Bauer 方法测量了处理过的织物对枯草杆菌微生物的抗菌活性。结果表明,处理过的织物对枯草杆菌具有抗菌活性,抑菌区为 8 毫米。对目标细菌的抗菌活性甚至在单次洗涤后仍然有效。光密度测试也证明了这一点,表明这种织物可用于保健 PPF,以确保其抗菌和抗病毒特性。
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来源期刊
Fibers and Polymers
Fibers and Polymers 工程技术-材料科学:纺织
CiteScore
3.90
自引率
8.00%
发文量
267
审稿时长
3.9 months
期刊介绍: -Chemistry of Fiber Materials, Polymer Reactions and Synthesis- Physical Properties of Fibers, Polymer Blends and Composites- Fiber Spinning and Textile Processing, Polymer Physics, Morphology- Colorants and Dyeing, Polymer Analysis and Characterization- Chemical Aftertreatment of Textiles, Polymer Processing and Rheology- Textile and Apparel Science, Functional Polymers
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