Mechanical, Microstructural and Wear Studies of a Ceramic Hybrid Reinforced ZE41 Magnesium Metal Matrix Composite Through Stir Casting Route

IF 2.6 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING International Journal of Metalcasting Pub Date : 2024-07-04 DOI:10.1007/s40962-024-01392-8
N. Anand, Senthil Kumaran Selvaraj
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Abstract

In this investigation, ZE41 magnesium alloys reinforced with 2% weight of SiC and B4C were manufactured through stir casting route under an inert environment. The microstructure of the unreinforced alloy, exhibits α Mg grains with uniformly distributed β Mg7Zn3 intermetallic phases at the grain boundaries. The addition of ceramic reinforcements decreased the average grain size and also formulated thin β Mg7Zn3 phases compared to the denser ones observed in the pure base matrix. The results of this work demonstrated that the tensile strength of the composites improved due to particle strengthening, grain refinement and presence of dislocations at the intermetallic regions and the best results were obtained for the hybrid ZE41 matrix (ZE41 + 2% SiC + 2% B4C). The tensile strengthening mechanisms of the composites are discussed and the expected theoretical values of yield strengths are calculated for comparison. Additionally, the specimens' elastic moduli were evaluated experimentally and theoretically (using the Tsai Halpin model), with the results showing good agreement, particularly for the hybrid composite. The morphologies of the fractured specimens were also analysed and it has been observed that the hybrid composite exhibited a ductile mode of fracture due to the presence of uniform dimples. The impact strength and hardness values of all the composites was also found experimentally and the best results were obtained for SiC and B4C composites which played a vital role in the selection of reinforcement particles for developing the hybrid composites. The wear analysis of the composites and their surface morphologies displayed considerable increase in friction coefficient and specific wear rate for hybrid composites at low and high loads.

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通过搅拌铸造工艺对陶瓷混合增强 ZE41 镁金属基复合材料进行力学、微结构和磨损研究
本研究在惰性环境下,通过搅拌铸造工艺制造了添加 2% SiC 和 B4C 的 ZE41 镁合金。未增强合金的微观结构表现为 α Mg 晶粒,晶界上均匀分布着 β Mg7Zn3 金属间相。添加陶瓷增强材料后,平均晶粒尺寸减小,β Mg7Zn3 相也变得稀疏,而纯基体中的β Mg7Zn3 相则更加致密。这项工作的结果表明,由于颗粒强化、晶粒细化和金属间区域位错的存在,复合材料的拉伸强度得到了提高,而混合 ZE41 基体(ZE41 + 2% SiC + 2% B4C)的结果最好。讨论了复合材料的拉伸强化机制,并计算了屈服强度的预期理论值,以进行比较。此外,还对试样的弹性模量进行了实验和理论评估(使用蔡-哈尔平模型),结果显示两者吻合良好,尤其是混合复合材料。此外,还对断裂试样的形态进行了分析,发现混合复合材料由于存在均匀的凹痕而呈现出韧性断裂模式。实验还发现了所有复合材料的冲击强度和硬度值,其中 SiC 和 B4C 复合材料的结果最好,这对选择开发混合复合材料的增强粒子起到了至关重要的作用。对复合材料及其表面形态进行的磨损分析表明,混合复合材料在低负荷和高负荷下的摩擦系数和特定磨损率都有显著增加。
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来源期刊
International Journal of Metalcasting
International Journal of Metalcasting 工程技术-冶金工程
CiteScore
4.20
自引率
42.30%
发文量
174
审稿时长
>12 weeks
期刊介绍: The International Journal of Metalcasting is dedicated to leading the transfer of research and technology for the global metalcasting industry. The quarterly publication keeps the latest developments in metalcasting research and technology in front of the scientific leaders in our global industry throughout the year. All papers published in the the journal are approved after a rigorous peer review process. The editorial peer review board represents three international metalcasting groups: academia (metalcasting professors), science and research (personnel from national labs, research and scientific institutions), and industry (leading technical personnel from metalcasting facilities).
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