Foaming‐structural relationship of rotational molded nanocomposite foams: Box–Behnken response surface methodology implementation

IF 3.1 4区 工程技术 Q2 POLYMER SCIENCE Polymers for Advanced Technologies Pub Date : 2024-07-06 DOI:10.1002/pat.6489
Mahsa Daryadel, Taher Azdast
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Abstract

Rotational molded foam is known as one of the most popular types of polymeric foams due to its unique properties. Hence, the production of rotational molded foam samples has been well‐addressed in the foam literature, and several researchers have tried to produce these samples using different approaches. However, there is no comprehensive research that investigates the structural properties of nanocomposite foam samples produced by a two‐step process of rotational molding and batch foaming. Therefore, the effect of nanoclay and foam processing parameters on the structural properties of the samples produced by this method was investigated in this study. For this purpose, the Box–Behnken design of response surface methodology was used. The results revealed that the foaming temperature was the most effective parameter on cell density and expansion ratio. Also, the foaming time was reported as the most effective parameter on the cell size. Then, the response variables were subjected to single‐ and multi‐objective optimizations. Finally, the addition of 1.2 wt% of nanoclay, the foaming temperature of 141°C, and the foaming time of 85 s were introduced as the most optimal conditions to simultaneously achieve maximum cell density and expansion ratio and minimum cell size in the rotational molded nanocomposite foam samples.
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旋转模塑纳米复合泡沫的发泡-结构关系:方框-贝肯响应面方法的实现
旋转模塑泡沫因其独特的性能而成为最受欢迎的聚合泡沫类型之一。因此,泡沫塑料文献对旋转模塑泡沫样品的生产进行了深入研究,一些研究人员尝试使用不同的方法生产这些样品。然而,目前还没有全面的研究来探讨通过旋转成型和批量发泡两步法生产的纳米复合泡沫样品的结构特性。因此,本研究调查了纳米粘土和泡沫加工参数对该方法生产的样品结构特性的影响。为此,采用了箱-贝肯响应面设计方法。结果表明,发泡温度是对细胞密度和膨胀率最有效的参数。此外,发泡时间也是对电池尺寸最有效的参数。然后,对响应变量进行了单目标和多目标优化。最后,1.2 wt%的纳米粘土添加量、141°C的发泡温度和85 s的发泡时间被认为是在旋转模塑纳米复合材料泡沫样品中同时获得最大孔密度和膨胀率以及最小孔尺寸的最佳条件。
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来源期刊
Polymers for Advanced Technologies
Polymers for Advanced Technologies 工程技术-高分子科学
CiteScore
6.20
自引率
5.90%
发文量
337
审稿时长
2.1 months
期刊介绍: Polymers for Advanced Technologies is published in response to recent significant changes in the patterns of materials research and development. Worldwide attention has been focused on the critical importance of materials in the creation of new devices and systems. It is now recognized that materials are often the limiting factor in bringing a new technical concept to fruition and that polymers are often the materials of choice in these demanding applications. A significant portion of the polymer research ongoing in the world is directly or indirectly related to the solution of complex, interdisciplinary problems whose successful resolution is necessary for achievement of broad system objectives. Polymers for Advanced Technologies is focused to the interest of scientists and engineers from academia and industry who are participating in these new areas of polymer research and development. It is the intent of this journal to impact the polymer related advanced technologies to meet the challenge of the twenty-first century. Polymers for Advanced Technologies aims at encouraging innovation, invention, imagination and creativity by providing a broad interdisciplinary platform for the presentation of new research and development concepts, theories and results which reflect the changing image and pace of modern polymer science and technology. Polymers for Advanced Technologies aims at becoming the central organ of the new multi-disciplinary polymer oriented materials science of the highest scientific standards. It will publish original research papers on finished studies; communications limited to five typewritten pages plus three illustrations, containing experimental details; review articles of up to 40 pages; letters to the editor and book reviews. Review articles will normally be published by invitation. The Editor-in-Chief welcomes suggestions for reviews.
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