Effects of the application protocol and bonding strategy of the universal adhesive on dentin previously impregnated with bioceramic sealer

IF 3.2 3区 材料科学 Q2 ENGINEERING, CHEMICAL International Journal of Adhesion and Adhesives Pub Date : 2024-07-13 DOI:10.1016/j.ijadhadh.2024.103765
Antonia Patricia Oliveira Barros , Joatan Lucas de Sousa Gomes Costa , Jardel Camilo do Carmo Monteiro , Lucas David Galvani , Marcelo Ferrarezi de Andrade , José Roberto Cury Saad , Milton Carlos Kuga
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Abstract

Purpose

To evaluate the effects of the application of universal adhesive with manual brush (MB) or rotary brush (RB), in the etch-and-rinse (ER) or self-etching (SE) strategy, on the bond strength, adhesive layer thickness, and adhesive failure pattern to dentin impregnated with bioceramic sealer, at 24 h and 1 year.

Materials and methods

Eighty-eight bovine incisor crowns were impregnated with bioceramic sealer was kept for 15 min and cleaned with cotton soaked in distilled water. They were then divided into four groups (n = 22): ER-MB, ER-RB, SE-MB, SE-RB. Subsequently, the specimens were restored with Filtek Z-250 resin. The adhesive layer thickness was individually analyzed using laser confocal microscope. Bond strength was assessed through microtensile testing, and the failure pattern was examined using a stereomicroscope. Data were analyzed by one-way ANOVA/Tukey's tests (α = 0.05).

Results

The adhesive layer thickness provided by ER-MB and SE-MB was greater than that provided by ER-RB and SE-RB (P < 0.05). ER-MB showed the lowest bond strength at 24 h (P < 0.05). At 1 year, SE-MB and SE-RB exhibited the highest bond strength values (P < 0.05). ER-MB demonstrated a higher incidence of adhesive failure at 24 h. At 1 year, SE-RB and SE-MB showed a higher incidence of mixed failure.

Conclusion

The use of Scotchbond Universal® adhesive in the etch-and-rinse strategy applied with a MB negatively affects bond strength at 24 h, worsening after 1 year of control, regardless of the application protocol.

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通用粘合剂的应用方案和粘接策略对先前浸渍过生物陶瓷封闭剂的牙本质的影响
材料和方法88颗牛门牙牙冠浸渍生物陶瓷封闭剂后保存15分钟,用棉花蘸蒸馏水清洗。然后将其分为四组(n = 22):ER-MB、ER-RB、SE-MB、SE-RB。随后,用 Filtek Z-250 树脂对试样进行修复。使用激光共聚焦显微镜对粘合层厚度进行单独分析。通过显微拉伸测试评估粘接强度,并使用体视显微镜检查破坏模式。结果 ER-MB 和 SE-MB 提供的粘合层厚度大于 ER-RB 和 SE-RB 提供的粘合层厚度(P < 0.05)。24 小时后,ER-MB 的粘接强度最低(P< 0.05)。1 年后,SE-MB 和 SE-RB 显示出最高的粘接强度值(P < 0.05)。24 小时后,ER-MB 显示出较高的粘合失效率;1 年后,SE-RB 和 SE-MB 显示出较高的混合失效率。结论在使用 MB 的蚀刻-冲洗策略中使用思高邦德 Universal® 粘合剂会对 24 小时后的粘合强度产生负面影响,并且在对照 1 年后会恶化,与使用协议无关。
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来源期刊
International Journal of Adhesion and Adhesives
International Journal of Adhesion and Adhesives 工程技术-材料科学:综合
CiteScore
6.90
自引率
8.80%
发文量
200
审稿时长
8.3 months
期刊介绍: The International Journal of Adhesion and Adhesives draws together the many aspects of the science and technology of adhesive materials, from fundamental research and development work to industrial applications. Subject areas covered include: interfacial interactions, surface chemistry, methods of testing, accumulation of test data on physical and mechanical properties, environmental effects, new adhesive materials, sealants, design of bonded joints, and manufacturing technology.
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