Temperature and strain rate-dependent compression properties of 3D-printed PLA: an experimental and modeling analysis

Shrushti Maheshwari, Anand Kumar, Pyaarjeet Singh Chaurasia, T. Niranjan, Zafar Alam, Sarthak S. Singh
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Abstract

Purpose This study aims to investigate the compression characteristics of the 3D-printed polylactic acid (PLA) samples at temperatures below the glass transition temperature (Tg) with varying strain rates and develop a thermo-mechanical viscoplastic constitutive model to predict the finite strain compression response using a single set of material parameters. Also, the micro-mechanical damage processes are linked to the global stress–strain response at varied strain rates and temperatures through scanning electron microscopy (SEM). Design/methodology/approach Tg of PLA was determined using a dynamic mechanical analyzer. Compression experiments were conducted at strain rates of 2 × 10–3/s and 2 × 10–2/s at 25°C, 40°C and 50°C. The failure mechanisms were examined using SEM. A finite strain thermo-mechanical viscoplastic constitutive model was developed to analyze the deformations at the considered strain rates and temperatures. Findings Tg of PLA was determined as 55°C. While the yield and post-yield stresses drop with increasing temperature, their trend reverses with an increased strain rate. SEM imaging indicated plasticizing effects at higher temperatures, while filament fragmentation and twisting at higher strain rates were identified as the dominant failure mechanisms. Using a non-linear regression analysis to predict the experimental data, an overall R2 value of 0.98 was achieved between experimental and model prediction, implying the robustness of the model’s calibration. Originality/value In this study, a viscoplastic constitutive model was developed that considers the combined effect of temperature and strain rate for FDM-printed PLA experiencing extensive compression. Using appropriate temperature-dependent modulus and flow rate properties, a single set of model parameters predicted the rise in the gap between yield stress and degree of softening as strain rates and temperatures increased.
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随温度和应变率变化的 3D 打印聚乳酸压缩特性:实验和建模分析
目的 本研究旨在调查三维打印聚乳酸(PLA)样品在低于玻璃化转变温度(Tg)的温度下不同应变速率下的压缩特性,并开发一种热机械粘塑性组成模型,以使用单组材料参数预测有限应变压缩响应。此外,还通过扫描电子显微镜(SEM)将微机械损伤过程与不同应变速率和温度下的整体应力-应变响应联系起来。在 25°C、40°C 和 50°C 下,以 2 × 10-3/s 和 2 × 10-2/s 的应变速率进行压缩实验。使用扫描电子显微镜检查了破坏机制。建立了有限应变热机械粘塑性构成模型,以分析在所考虑的应变速率和温度下的变形。虽然屈服应力和屈服后应力随温度升高而下降,但其趋势随着应变速率的增加而逆转。扫描电子显微镜成像显示,在较高温度下会产生塑化效应,而在较高应变速率下,长丝断裂和扭曲被认为是主要的失效机制。使用非线性回归分析预测实验数据,实验和模型预测之间的总体 R2 值达到 0.98,这意味着模型校准的稳健性。利用适当的温度相关模量和流速特性,一套模型参数就能预测屈服应力与软化程度之间的差距会随着应变率和温度的增加而增大。
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