Enhancement the physical properties of V2O5/Ni0.1Fe2.9O4 nanocomposite

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS Journal of the Australian Ceramic Society Pub Date : 2024-07-15 DOI:10.1007/s41779-024-01051-5
Rania Ramadan
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Abstract

Nanocomposite containing vanadium oxide (V2O5) and magnetite (Fe3O4) doped with nickel (Ni) ion were synthesized according to the formula of Ni0.1Fe2.9O4 /V2O5. The obtained composition was characterized by XRD, FTIR, FESEM. The FESEM micrograph shows that the existence of two different phases related to V2O5 and Ni-Magnetite. Moreover,the roughness parameters have values of 281, 85 and 385nm for roughness average Ra, root mean square roughness Rq, Maximum height of roughness RT respectively. Moreover, the magnetic behavior of the sample was studied, and we found that by adding V2O5 to Ni dopped magnetite, the curie temperature value was lowered from 750 oC to 625 oC. The activation energy was calculated and found to be 0.22 eV and 0.08 eV for 1000 Hz and 3MHz respectively.

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增强 V2O5/Ni0.1Fe2.9O4 纳米复合材料的物理性质
根据Ni0.1Fe2.9O4 /V2O5的分子式合成了含钒(V2O5)和掺杂镍(Ni)离子的磁铁矿(Fe3O4)的纳米复合材料。采用XRD、FTIR、FESEM对所得成分进行了表征。FESEM显微形貌分析表明,试样中存在与V2O5和ni -磁铁矿相关的两种相。粗糙度平均值Ra、均方根粗糙度Rq、最大粗糙度高度RT分别为281、85和385nm。此外,对样品的磁性行为进行了研究,发现在Ni掺杂的磁铁矿中加入V2O5,使样品的居里温度从750℃降低到625℃。在1000 Hz和3MHz下,计算得到的活化能分别为0.22 eV和0.08 eV。
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来源期刊
Journal of the Australian Ceramic Society
Journal of the Australian Ceramic Society Materials Science-Materials Chemistry
CiteScore
3.70
自引率
5.30%
发文量
123
期刊介绍: Publishes high quality research and technical papers in all areas of ceramic and related materials Spans the broad and growing fields of ceramic technology, material science and bioceramics Chronicles new advances in ceramic materials, manufacturing processes and applications Journal of the Australian Ceramic Society since 1965 Professional language editing service is available through our affiliates Nature Research Editing Service and American Journal Experts at the author''s cost and does not guarantee that the manuscript will be reviewed or accepted
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