Scanning Acoustic Microscopy Characterization of Cold-Sprayed Coatings Deposited on Grooved Substrates

IF 3.2 3区 材料科学 Q2 MATERIALS SCIENCE, COATINGS & FILMS Journal of Thermal Spray Technology Pub Date : 2024-07-16 DOI:10.1007/s11666-024-01806-3
Martin Koller, Jan Cizek, Michaela Janovská, Martin Ševčík, Jan Kondas, Reeti Singh, Hanuš Seiner
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Abstract

The effect of non-planar substrate surface on homogeneity and quality of cold-sprayed (CS) deposits was studied by scanning acoustic microscopy (SAM). Fe coatings were cold-sprayed onto Al substrates containing artificially introduced grooves of square- and trapezoid-shaped geometries, with flat or cylindrical bottoms. The Al substrates were either wrought or cold-sprayed, to comprehend their prospective influence on the Fe coatings buildup. SAM was then used to assess morphological properties of the materials from the cross-view and top-view directions. The microstructure below the surface of the studied samples was visualized by measuring the amplitudes of the reflection echoes and the velocity of the ultrasonic waves. The SAM analysis revealed that the regions of coating imperfections around the grooves are larger than what is suggested by standard scanning electron microscopy (SEM) observations. Furthermore, we found that the seemingly non-influenced coating regions that appear perfectly homogeneous and dense in SEM do, in fact, possess heterogeneous microstructure associated with the individual CS nozzle passes.

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扫描声学显微镜表征沉积在凹槽基底上的冷喷涂层
通过扫描声学显微镜(SAM)研究了非平面基底表面对冷喷(CS)镀层的均匀性和质量的影响。铁涂层被冷喷涂在铝基底上,铝基底上有人工引入的方形和梯形凹槽,底部为平面或圆柱形。铝基板经过锻造或冷喷,以了解其对铁涂层形成的预期影响。然后使用 SAM 从横向和纵向评估材料的形态特性。通过测量反射回波的振幅和超声波的速度,可以观察到所研究样品表面下的微观结构。SAM 分析表明,凹槽周围的涂层缺陷区域比标准扫描电子显微镜 (SEM) 观察到的要大。此外,我们还发现,在扫描电子显微镜下看似完全均匀致密的无影响涂层区域,实际上具有与单个 CS 喷嘴通过相关的异质微观结构。
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来源期刊
Journal of Thermal Spray Technology
Journal of Thermal Spray Technology 工程技术-材料科学:膜
CiteScore
5.20
自引率
25.80%
发文量
198
审稿时长
2.6 months
期刊介绍: From the scientific to the practical, stay on top of advances in this fast-growing coating technology with ASM International''s Journal of Thermal Spray Technology. Critically reviewed scientific papers and engineering articles combine the best of new research with the latest applications and problem solving. A service of the ASM Thermal Spray Society (TSS), the Journal of Thermal Spray Technology covers all fundamental and practical aspects of thermal spray science, including processes, feedstock manufacture, and testing and characterization. The journal contains worldwide coverage of the latest research, products, equipment and process developments, and includes technical note case studies from real-time applications and in-depth topical reviews.
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