Dynamic bending analysis of metallized silicon nitride substrate during thermal cycling via digital image correlation

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS International Journal of Applied Ceramic Technology Pub Date : 2024-07-23 DOI:10.1111/ijac.14875
Minh Chu Ngo, Hiroyuki Miyazaki, Kiyoshi Hirao, Tatsuki Ohji, Manabu Fukushima
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Abstract

Digital image correlation (DIC) method was employed to analyze the dynamic bending of a metallized Si3N4 substrate in thermal cycles ranging from −40°C to 250°C. The substrate was monitored by DIC over several consecutive cycles, spanning from 0 to 2501. Three DIC measurement intervals, specifically during 999–1001, 1999–2001, and 2499–2501 cycles, were selected to analyze the bending behavior in response to temperature fluctuations. By the scanning acoustic microscope (SAM), the substrate revealed negligible delamination after 1001 cycles, light delamination after 2001 cycles, and serious delamination post‐2501 cycles. The dynamic bending remained unchanged during 999–1001 cycles. A curve with a negative bending was observed during 1999–2001 cycles, with a peak curvature of .024 mm−1 at −40°C; the negative bending intensified with a curvature reaching .050 mm−1 at −40°C during 2499–2501 cycles. The bending curve then decreased during the heating phase and returned to a non‐bent state at elevated temperatures. The bending curve reversed to positive at 250°C during thermal cycles from 2499 to 2501. The bending behavior throughout thermal cycles was discussed in relation to the asymmetric delamination observed on both sides of the substrate, as well as the distribution of delamination.
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通过数字图像关联分析氮化硅金属化基板在热循环过程中的动态弯曲情况
采用数字图像相关(DIC)方法分析了金属化 Si3N4 衬底在 -40°C 至 250°C 的热循环中的动态弯曲情况。基片在 0 至 2501 的几个连续循环中受到 DIC 的监测。选择了三个 DIC 测量间隔,特别是在 999-1001、1999-2001 和 2499-2501 个循环期间,以分析弯曲行为对温度波动的响应。通过扫描声学显微镜 (SAM),基底在 1001 次循环后出现可忽略不计的分层,2001 次循环后出现轻度分层,2501 次循环后出现严重分层。在 999-1001 次循环期间,动态弯曲保持不变。在 1999-2001 次循环期间,观察到一条负弯曲曲线,在 -40°C 时的曲率峰值为 0.024 mm-1;在 2499-2501 次循环期间,负弯曲加剧,在 -40°C 时的曲率达到 0.050 mm-1。在加热阶段,弯曲曲线随之减小,并在高温下恢复到无弯曲状态。在 2499 至 2501 次热循环期间,弯曲曲线在 250°C 时反转为正值。讨论了整个热循环期间的弯曲行为与基材两侧观察到的不对称分层以及分层分布的关系。
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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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