Supercritical CO2 Extraction of Natural Compounds from Capuchin (Tropaeolum majus) Leaves and Seeds

Processes Pub Date : 2024-07-26 DOI:10.3390/pr12081566
Gabriel Corrêa, Michel Rubens dos Reis Souza, Eduardo Soares Nascimento, Thiago Rodrigues Bjerk, José Eduardo Gonçalves, Cristiane Mengue Feniman Moritz, Ó. A. Sakai, Erivaldo Antônio da Silva, R. J. Santos, Edson Antônio da Silva, Lúcio Cardozo-Filho, A. Zanette, L. Ferreira-Pinto
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Abstract

This study investigated the supercritical CO2 extraction of oils from capuchin (Tropaeolum majus) seeds (4.34% moisture content) and leaves (5.26% moisture content) and analyzed the effects of varying temperature and pressure conditions. The extraction yields were 3% for the seeds and 2% for the leaves. The seed extracts were rich in oleic, linoleic, and palmitic fatty acids, whereas the leaf extracts contained a high concentration of octacosanol (73.37%). Kinetic analysis revealed distinct mass transfer mechanisms during extraction, and the Sovová model effectively described the extraction kinetics, showing good agreement with experimental data (ADD% < 4%). An analysis of variance (ANOVA) demonstrated the impact of temperature and pressure on the yields, with temperature being the most influential factor. The experimental conditions ranged from 22 to 28 MPa and from 313.15 to 333.15 K. This study contributes to the understanding of capuchin oil extraction and its potential applications in various fields, owing to the presence of bioactive compounds.
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超临界二氧化碳萃取毛果芸香(Tropaeolum majus)叶片和种子中的天然化合物
本研究调查了从毛果芸香(Tropaeolum majus)种子(含水量为 4.34%)和叶片(含水量为 5.26%)中超临界二氧化碳萃取油脂的情况,并分析了不同温度和压力条件的影响。种子和叶片的提取率分别为 3% 和 2%。种子提取物富含油酸、亚油酸和棕榈脂肪酸,而叶片提取物则含有高浓度的二十八烷醇(73.37%)。动力学分析揭示了萃取过程中不同的传质机制,索沃瓦模型有效地描述了萃取动力学,与实验数据(ADD% < 4%)显示出良好的一致性。方差分析(ANOVA)显示了温度和压力对产量的影响,其中温度是影响最大的因素。实验条件从 22 到 28 兆帕,从 313.15 到 333.15 K。这项研究有助于了解卷尾猴油提取及其在各个领域的潜在应用,因为其中含有生物活性化合物。
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