Manufacturing of Al-Zr-Si master alloy from zircon concentrate

Huynh Cong Khanh, Ly Thai Phap, Do Thanh Toan
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Abstract

Aluminum alloy of thermal-resistant aluminum alloy wire for overhead line conductors usually contains zirconium, silicon, iron, and other components. Hence, Al-Zr-Si master alloy can be used to produce thermal-resistant aluminum alloy. In this study, the manufacturing procedure of Al-Zr-Si master alloy from zircon concentrate has been introduced. The zircon concentrate was thoroughly mixed with different amounts of KCl and Na2SiF6 or Na3AlF6, then sintered in the electric muffle furnace at 700oC for 2 hrs with automatic temperature control. The sinter was premixed with Na3­AlF6 at the 1:1 ratio and dried at 140-160oC to remove the humidity. The powder mixture was added to the aluminum molten at 1200o­C and then stirred well to ensure proper powder mixing in the melt. After the finish reaction and slag skimming, the melt was taken out of the furnace and poured into the mold. The master alloy was characterized by a Spectrometer, ICP-OES, and optical microscopy.
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利用锆石精矿制造铝-锆-硅母合金
用于架空线路导体的耐热铝合金线的铝合金通常含有锆、硅、铁和其他成分。因此,Al-Zr-Si 母合金可用于生产耐热铝合金。本研究介绍了利用锆石精矿制造 Al-Zr-Si 母合金的程序。将锆石精矿与不同量的 KCl 和 Na2SiF6 或 Na3AlF6 充分混合,然后在自动控温的情况下于 700oC 的电马弗炉中烧结 2 小时。烧结料与 Na3AlF6 按 1:1 的比例预混合,并在 140-160oC 下烘干以去除湿气。将粉末混合物加入 1200 摄氏度的铝熔液中,然后充分搅拌,以确保粉末在熔液中充分混合。完成反应和撇渣后,熔体从熔炉中取出并倒入模具中。使用光谱仪、ICP-OES 和光学显微镜对母合金进行表征。
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