Sofia G Gomez , Dale Cillessen , Jonathon Duay , Kevin Strong , Katrina Sadzewicz , Eric MacDonald
{"title":"Tracking the chemical composition of 3D printed 94 % alumina during the thermal post-process","authors":"Sofia G Gomez , Dale Cillessen , Jonathon Duay , Kevin Strong , Katrina Sadzewicz , Eric MacDonald","doi":"10.1016/j.addlet.2024.100225","DOIUrl":null,"url":null,"abstract":"<div><p>Additive manufactured (AM) 94 % alumina was successfully 3D printed using the Lithography Ceramic Manufacturing (LCM) technique. Each 3D printed sample was exposed to a different stage of the thermal post-process to identify changes in chemical composition at each stage. The thermal phases studied were the as printed green state, preconditioning at 120 °C, debinding at 600 °C, debinding at 1100 °C, and sintering at 1650 °C. Fourier Transform Infrared Spectroscopy (FTIR), Raman Spectroscopy, Thermogravimetric Analysis (TGA), and X-Ray Fluorescence (XRF) were used to evaluate the changes in composition at each stage of the thermal post-process. Cross-sectional images of 3D printed alumina samples after thermal exposure were captured using scanning electron microscopy (SEM).</p></div>","PeriodicalId":72068,"journal":{"name":"Additive manufacturing letters","volume":"10 ","pages":"Article 100225"},"PeriodicalIF":4.2000,"publicationDate":"2024-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2772369024000331/pdfft?md5=91eb267da2e9f7fc88092dd888e78d85&pid=1-s2.0-S2772369024000331-main.pdf","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Additive manufacturing letters","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S2772369024000331","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"ENGINEERING, MANUFACTURING","Score":null,"Total":0}
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Abstract
Additive manufactured (AM) 94 % alumina was successfully 3D printed using the Lithography Ceramic Manufacturing (LCM) technique. Each 3D printed sample was exposed to a different stage of the thermal post-process to identify changes in chemical composition at each stage. The thermal phases studied were the as printed green state, preconditioning at 120 °C, debinding at 600 °C, debinding at 1100 °C, and sintering at 1650 °C. Fourier Transform Infrared Spectroscopy (FTIR), Raman Spectroscopy, Thermogravimetric Analysis (TGA), and X-Ray Fluorescence (XRF) were used to evaluate the changes in composition at each stage of the thermal post-process. Cross-sectional images of 3D printed alumina samples after thermal exposure were captured using scanning electron microscopy (SEM).
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