Production and Characterization of Zn1 – xFexS Thin Films by Ultrasonic Chemical Spray Deposition Technique

IF 0.9 4区 物理与天体物理 Q4 PHYSICS, CONDENSED MATTER Physics of the Solid State Pub Date : 2024-08-07 DOI:10.1134/s1063783424600857
Tuba Solakyildirim, Umit Alver
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Abstract

In this study, Zn1 – xFexS thin films were synthesized using the chemical spray pyrolysis technique at a substrate temperature of 450°C and with varying Fe concentrations. The spraying solution was prepared by combining distilled water with 0.05 M zinc chloride (ZnCl2), 0.05 M iron chloride (FeCl3⋅6H2O), and 0.2 M thiourea ((NH2)2CS). The initial solution was atomized onto heated glass substrates using an ultrasonic nebulizer operating at a frequency of 1.63 MHz and dry air. The morphology of the films was examined by scanning electron microscopy (SEM). The crystal structures were determined by X-ray diffraction analysis (XRD). The optical properties of the films were analyzed using a UV spectrometer. The energy band gap of the films was defined using the absorption spectrum.

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利用超声波化学喷雾沉积技术制备 Zn1 - xFexS 薄膜并确定其特性
摘要 本研究采用化学喷雾热解技术,在 450°C 的基底温度和不同的铁浓度下合成了 Zn1 - xFexS 薄膜。喷射溶液由蒸馏水与 0.05 M 氯化锌 (ZnCl2)、0.05 M 氯化铁 (FeCl3⋅6H2O) 和 0.2 M 硫脲 ((NH2)2CS)混合配制而成。使用频率为 1.63 MHz 的超声雾化器和干燥空气将初始溶液雾化到加热的玻璃基底上。薄膜的形态由扫描电子显微镜(SEM)进行检测。通过 X 射线衍射分析 (XRD) 确定了晶体结构。使用紫外光谱仪分析了薄膜的光学特性。利用吸收光谱确定了薄膜的能带隙。
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来源期刊
Physics of the Solid State
Physics of the Solid State 物理-物理:凝聚态物理
CiteScore
1.70
自引率
0.00%
发文量
60
审稿时长
2-4 weeks
期刊介绍: Presents the latest results from Russia’s leading researchers in condensed matter physics at the Russian Academy of Sciences and other prestigious institutions. Covers all areas of solid state physics including solid state optics, solid state acoustics, electronic and vibrational spectra, phase transitions, ferroelectricity, magnetism, and superconductivity. Also presents review papers on the most important problems in solid state physics.
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