The distribution of Y2O3 during selective laser melting of IN625/Y2O3 core-shell powders

IF 4.2 2区 工程技术 Q2 ENGINEERING, CHEMICAL Advanced Powder Technology Pub Date : 2024-08-06 DOI:10.1016/j.apt.2024.104609
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Abstract

Selective laser melting (SLM) of metal-oxide hybrid powder is currently a cost-effective approach for fabricating oxide-dispersion-strengthened alloys. The distribution behavior of oxide during the SLM process has significant effects on the performance of the final components. In this work, Y2O3 strengthened IN625 superalloys were fabricated by selective laser melting using IN625 powder coated by 1 wt% and 3 wt% Y2O3. The hybrid powder prepared by the resonant mixing method present the good flowability. Due to the high melting point of Y2O3 powder and its harmful effect on the wettability between the melt track and the formed surface, the required laser energy density for successful SLM-fabrication of the hybrid powder should be high. The distribution characteristics of Y2O3 during the SLM process and the corresponding evolution mechanism were analyzed. It was found that severe loss of Y2O3 occurred during SLM process, resulting from Y2O3 slag on the top surface of the built specimen, Y2O3 adhered to spatter particles falling into the recycling powder, and Y2O3 plume blown into the machine filter by the gas flow. The more Y2O3 coated on the metal powder, the more Y2O3 lost during SLM. The molten pool with keyhole mode is favorable to reduce Y2O3 loss compared to the conduction mode.

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选择性激光熔融 IN625/Y2O3 核壳粉末过程中 Y2O3 的分布
金属氧化物混合粉末的选择性激光熔融(SLM)是目前制造氧化物分散强化合金的一种经济有效的方法。在 SLM 过程中,氧化物的分布行为对最终部件的性能有重大影响。在这项工作中,使用涂有 1 wt% 和 3 wt% Y2O3 的 IN625 粉末,通过选择性激光熔融制造了 Y2O3 强化 IN625 超合金。共振混合法制备的混合粉末具有良好的流动性。由于 Y2O3 粉末的熔点较高,且其对熔体轨道和成型表面之间的润湿性有不利影响,因此要成功地用 SLM 制造混合粉末,所需的激光能量密度必须较高。研究分析了 Y2O3 在 SLM 过程中的分布特征以及相应的演变机制。研究发现,在 SLM 过程中,Y2O3 损失严重,这主要是由于 Y2O3 熔渣附着在制备好的试样顶面上,Y2O3 附着在溅射颗粒上落入回收粉末中,以及 Y2O3 烟羽被气流吹入机器过滤器。金属粉末上附着的 Y2O3 越多,SLM 过程中损失的 Y2O3 就越多。与传导模式相比,带锁孔模式的熔池有利于减少 Y2O3 的损失。
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来源期刊
Advanced Powder Technology
Advanced Powder Technology 工程技术-工程:化工
CiteScore
9.50
自引率
7.70%
发文量
424
审稿时长
55 days
期刊介绍: The aim of Advanced Powder Technology is to meet the demand for an international journal that integrates all aspects of science and technology research on powder and particulate materials. The journal fulfills this purpose by publishing original research papers, rapid communications, reviews, and translated articles by prominent researchers worldwide. The editorial work of Advanced Powder Technology, which was founded as the International Journal of the Society of Powder Technology, Japan, is now shared by distinguished board members, who operate in a unique framework designed to respond to the increasing global demand for articles on not only powder and particles, but also on various materials produced from them. Advanced Powder Technology covers various areas, but a discussion of powder and particles is required in articles. Topics include: Production of powder and particulate materials in gases and liquids(nanoparticles, fine ceramics, pharmaceuticals, novel functional materials, etc.); Aerosol and colloidal processing; Powder and particle characterization; Dynamics and phenomena; Calculation and simulation (CFD, DEM, Monte Carlo method, population balance, etc.); Measurement and control of powder processes; Particle modification; Comminution; Powder handling and operations (storage, transport, granulation, separation, fluidization, etc.)
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