Optimizing SEM parameters for segmentation with AI – Part 1: Generating a training set

IF 3.1 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Computational Materials Science Pub Date : 2024-08-15 DOI:10.1016/j.commatsci.2024.113255
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Abstract

Extracting significant quantitative results from SEM images requires feature segmentation with image processing software. The efficiency of segmentation algorithms depends on the image quality, determined by the parameters set on the microscope during acquisitions. By integrating AI within SEM acquisition workflows, it is possible to suggest microscope parameters that will produce images where the features to quantify will be easily segmented. Specifically, a model is trained to automatically suggest the beam energy and probe current to set on the microscope during acquisitions. This paper is the first of two parts, describing workflows for generating a complete training set. The training set is carefully designed, consisting of both simulated data and real data acquired on the SEM by varying the energy and current. Separate workflows are required for generating simulated and acquired training examples. Simulated data generation is accomplished with the MC X-ray simulator in Dragonfly, where multiple virtual samples are created to intentionally diversify the training set. Acquiring data on the SEM for training is a time-consuming process when compared to generating simulations and would ideally be avoided but is included here to determine the degree to which it is required. Using only simulated data for adequate training, we show that our data generation workflow can be fully automated and produces a considerable amount of high quality data rapidly and with minimal effort.

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利用人工智能优化 SEM 参数以进行细分 - 第 1 部分:生成训练集
从扫描电镜图像中提取重要的定量结果需要使用图像处理软件进行特征分割。分割算法的效率取决于图像质量,而图像质量由采集时显微镜上设置的参数决定。通过将人工智能集成到 SEM 采集工作流程中,可以建议显微镜参数,从而生成易于分割量化特征的图像。具体来说,通过对模型进行训练,可自动建议采集期间在显微镜上设置的光束能量和探针电流。本文分为两部分,第一部分介绍了生成完整训练集的工作流程。训练集经过精心设计,包括模拟数据和通过改变能量和电流在扫描电镜上获取的真实数据。生成模拟和获取的训练示例需要不同的工作流程。模拟数据的生成是通过 Dragonfly 中的 MC X 射线模拟器完成的,其中创建了多个虚拟样本,以有意识地使训练集多样化。与生成模拟数据相比,在扫描电子显微镜上获取数据进行训练是一个耗时的过程,理想情况下可以避免,但在此也包括在内,以确定需要的程度。我们仅使用模拟数据进行了充分的训练,结果表明我们的数据生成工作流程可以完全自动化,并能以最小的工作量快速生成大量高质量数据。
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来源期刊
Computational Materials Science
Computational Materials Science 工程技术-材料科学:综合
CiteScore
6.50
自引率
6.10%
发文量
665
审稿时长
26 days
期刊介绍: The goal of Computational Materials Science is to report on results that provide new or unique insights into, or significantly expand our understanding of, the properties of materials or phenomena associated with their design, synthesis, processing, characterization, and utilization. To be relevant to the journal, the results should be applied or applicable to specific material systems that are discussed within the submission.
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