Effect of Lipid-soluble rosemary (Rosmarinus Officinalis L.) extract (carnosic acid) on properties of microcrystalline cellulose/corn starch composite films

Na Yang , Haojie Sha , Wenlu Bi , Sheng Li , Shusong Wu , Dingding Su
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Abstract

The development of biodegradable bioactive films is crucial due to the environmental pollution caused by petroleum-based materials and the food spoilage. Microcrystalline cellulose (MCC)/corn starch (CS) composite films containing lipid-soluble rosemary extract (carnosic acid) (RE) (1 %∼7 %, w/w) were prepared and the effect of RE on the structural, physicochemical, antimicrobial and antioxidant properties of MCC/CS composite films was investigated. The incorporation of lower RE content (1 %) promoted the interactions between film components, thus forming a compact and smooth surface and cross structures. The incorporation of RE changed the long-range order structure of MCC/CS composite film, strengthened the intermolecular interaction between film components, and improved thermal stability. The tensile strength increased from 8.35 MPa to 10.53 MPa and the water vapor permeability decreased from 0.63 to 0.58 g.mm.h-1.m-2.KPa-1. Moreover. Antibacterial (Escherichia coli and Staphylococcus aureus) and antioxidant activity were upsurged as RE contents increased. TOPSIS method indicated the MCC/CS-3 % film and MCC/CS-5 % film were the best films. The above results indicated that an effective use of RE as an enhancer and bacteriostatic agent showed a promising application in food packaging.

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脂溶性迷迭香(Rosmarinus Officinalis L.)提取物(肉毒碱)对微晶纤维素/玉米淀粉复合薄膜性能的影响
由于石油基材料造成的环境污染和食品腐败,开发可生物降解的生物活性薄膜至关重要。本研究制备了含有脂溶性迷迭香提取物(肉毒碱)(RE)(1 %∼7 %,w/w)的微晶纤维素(MCC)/玉米淀粉(CS)复合薄膜,并研究了 RE 对 MCC/CS 复合薄膜的结构、理化、抗菌和抗氧化性能的影响。较低 RE 含量(1%)的加入促进了薄膜成分之间的相互作用,从而形成了紧凑光滑的表面和交叉结构。RE 的加入改变了 MCC/CS 复合薄膜的长程有序结构,增强了薄膜组分间的分子间相互作用,提高了热稳定性。拉伸强度从 8.35 MPa 提高到 10.53 MPa,水蒸气渗透率从 0.63 g.mm.h-1.m-2.KPa-1 降低到 0.58 g.mm.h-1.m-2.KPa-1。此外。抗菌(大肠杆菌和金黄色葡萄球菌)和抗氧化活性随着 RE 含量的增加而提高。TOPSIS 方法表明,MCC/CS-3 % 薄膜和 MCC/CS-5 % 薄膜是最佳薄膜。上述结果表明,有效利用 RE 作为增效剂和抑菌剂在食品包装中的应用前景广阔。
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