Improved precision and mechanical properties of 3D‐printed silica ceramics via sintering temperature optimization

IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS International Journal of Applied Ceramic Technology Pub Date : 2024-08-16 DOI:10.1111/ijac.14880
Yunsong Mu, Yanhua Chen, He Li, Jingwen Sun, Baoxia Mu, Paolo Colombo
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Abstract

Ceramic cores are the key components of precision casting hollow turbine blades, and 3D‐printed silica‐based ceramic cores are crucial to the development of the aerospace industry. However, silica‐based ceramic cores have problems in terms of mechanical properties and friction properties. In this paper, silica ceramics were prepared by stereolithography‐based 3D printing technology and processed at different sintering temperatures. The effect of sintering temperature on the microstructure, physical–mechanical properties, and friction and wear properties of the silica ceramics was investigated. The results show that, with the increase of sintering temperature, the average particle size and bulk density of the samples increased, while the open porosity and layer thickness decreased. The surface of ceramics became more and more flat with the increase in temperature. The flexural strength first increased with increasing temperature, and then suddenly decreased at 1350°C. The average surface roughness decreased with increasing temperature. The wear of the material decreased with increasing sintering temperature and increased at 1350°C. The optimum sintering temperatures were 1250°C and 1300°C, giving a flexural strength of 23.18 and 23.25 MPa, bulk density of 1.72 and 1.78 g/cm3, and open porosity of 24.49% and 23.66%, respectively.
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通过优化烧结温度提高 3D 打印硅陶瓷的精度和机械性能
陶瓷芯是精密铸造空心涡轮叶片的关键部件,而三维打印硅基陶瓷芯对航空航天工业的发展至关重要。然而,硅基陶瓷芯在机械性能和摩擦性能方面存在问题。本文采用基于立体光刻技术的三维打印技术制备了二氧化硅陶瓷,并在不同的烧结温度下进行了处理。研究了烧结温度对二氧化硅陶瓷的微观结构、物理机械性能以及摩擦和磨损性能的影响。结果表明,随着烧结温度的升高,样品的平均粒度和体积密度增大,而开孔率和层厚度减小。陶瓷表面随着温度的升高变得越来越平整。抗折强度先是随着温度的升高而增加,然后在 1350°C 时突然下降。平均表面粗糙度随温度升高而降低。材料的磨损随着烧结温度的升高而减小,并在 1350°C 时增大。最佳烧结温度为 1250°C 和 1300°C,其抗弯强度分别为 23.18 和 23.25 兆帕,体积密度分别为 1.72 和 1.78 克/立方厘米,开孔率分别为 24.49% 和 23.66%。
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来源期刊
International Journal of Applied Ceramic Technology
International Journal of Applied Ceramic Technology 工程技术-材料科学:硅酸盐
CiteScore
3.90
自引率
9.50%
发文量
280
审稿时长
4.5 months
期刊介绍: The International Journal of Applied Ceramic Technology publishes cutting edge applied research and development work focused on commercialization of engineered ceramics, products and processes. The publication also explores the barriers to commercialization, design and testing, environmental health issues, international standardization activities, databases, and cost models. Designed to get high quality information to end-users quickly, the peer process is led by an editorial board of experts from industry, government, and universities. Each issue focuses on a high-interest, high-impact topic plus includes a range of papers detailing applications of ceramics. Papers on all aspects of applied ceramics are welcome including those in the following areas: Nanotechnology applications; Ceramic Armor; Ceramic and Technology for Energy Applications (e.g., Fuel Cells, Batteries, Solar, Thermoelectric, and HT Superconductors); Ceramic Matrix Composites; Functional Materials; Thermal and Environmental Barrier Coatings; Bioceramic Applications; Green Manufacturing; Ceramic Processing; Glass Technology; Fiber optics; Ceramics in Environmental Applications; Ceramics in Electronic, Photonic and Magnetic Applications;
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