Probing the limits of tetraalkylthiuram disulfide synthesis by direct reaction of secondary amines with CS2: The structures of Cy2NC(S)SSC(S)NCy2 and Cy2NC(S)SSSSC(S)NCy2
Saikat Mishra, Gayathri Ragunathan, Joel T. Mague, Xiaodong Zhang, James P. Donahue
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引用次数: 0
Abstract
Reaction of Cy2NH with CS2 in NaOH/H2O, followed by oxidation with I2, yields a complex mixture that includes the tetracyclohexylthiuram disulfide, Cy2NC(S)SSC(S)NCy2, in mixture with S8 and the te...
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