Microstructural analysis and defect characterization of additively manufactured AA6061 aluminum alloy via laser powder bed fusion

IF 11.2 1区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Science & Technology Pub Date : 2024-09-24 DOI:10.1016/j.jmst.2024.08.056
Sivaji Karna, Lang Yuan, Tianyu Zhang, Rimah Al-Aridi, Andrew J. Gross, Daniel Morrall, Timothy Krentz, Dale Hitchcock
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Abstract

AA6061 is a widely used aluminum alloy with significant applications in the aerospace and automotive industries. Despite its popularity, the utilization of additively manufactured AA6061 through the laser powder bed fusion (LPBF) process has been hindered by the pronounced formation of pores and cracks during rapid solidification. This study quantitatively investigated defects, including pores and cracks, and microstructures, including texture, grain size, subgrain structure, and precipitates, of LPBF-manufactured AA6061 across a broad spectrum of laser power and speed combinations. A high relative density of more than 99 % was achieved with a low-power and low-speed condition, specifically 200 W and 100 mm/s, with minimal cracks. Large pores, akin to or exceeding melt pool dimensions, emerged under either low or high energy densities, driven by the lack of fusion and vaporization/denudation mechanisms, respectively. Solidification cracks, confirmed by the fractography, were propagated along grain boundaries and are highly dependent on laser scanning speed. Elevated power and speed exhibited finer grain size with refined subgrain cellular structures and increased precipitates at interdendritic regions. The cooling rate and thermal gradient estimated from thermal analytical solutions explain the microstructures’ characteristics. Nano-sized Si-Fe-Mg enriched precipitates are confirmed in both as-built and heat-treated conditions, whereas T6 heat treatment promotes a uniform distribution with coarsening of those precipitates. The low-power and low-speed conditions demonstrated the highest yield strength, consistent with defect levels. A minimum of 102.3 % increase in yield strength with reduced ductility was observed after heat treatment for all examined conditions. This work sheds light on printing parameters to mitigate the formation of pores and cracks in additively manufactured AA6061, proposing a process window for optimized fabrication and highlighting the potential for enhanced material properties and reduced defects through process control.

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通过激光粉末床熔融快速成型 AA6061 铝合金的微结构分析和缺陷表征
AA6061 是一种广泛使用的铝合金,在航空航天和汽车行业有着重要的应用。尽管 AA6061 很受欢迎,但由于其在快速凝固过程中会形成明显的气孔和裂纹,通过激光粉末床熔化(LPBF)工艺添加制造的 AA6061 的使用一直受到阻碍。本研究定量研究了 LPBF 制造的 AA6061 在各种激光功率和速度组合下的缺陷(包括气孔和裂纹)和微观结构(包括纹理、晶粒尺寸、亚晶粒结构和析出物)。在低功率和低速条件下(具体为 200 W 和 100 mm/s),相对密度高达 99 % 以上,裂纹极少。在低能量密度或高能量密度条件下,由于缺乏熔融和汽化/沉降机制,出现了类似或超过熔池尺寸的大气孔。碎裂图证实,凝固裂纹沿着晶界传播,与激光扫描速度密切相关。功率和速度的提高会使晶粒尺寸更细,亚晶粒蜂窝结构更精细,树枝间区域的沉淀物增多。从热分析溶液中估算出的冷却速率和热梯度解释了微结构的特征。纳米级的硅-铁-镁富集析出物在坯料和热处理条件下都得到了证实,而 T6 热处理则促进了这些析出物的均匀分布和粗化。低功率和低速条件下的屈服强度最高,与缺陷水平一致。在所有检查条件下,热处理后的屈服强度最低提高了 102.3%,但延展性有所降低。这项研究揭示了可减轻添加式制造 AA6061 中气孔和裂纹形成的印刷参数,提出了优化制造的工艺窗口,并强调了通过工艺控制提高材料性能和减少缺陷的潜力。
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来源期刊
Journal of Materials Science & Technology
Journal of Materials Science & Technology 工程技术-材料科学:综合
CiteScore
20.00
自引率
11.00%
发文量
995
审稿时长
13 days
期刊介绍: Journal of Materials Science & Technology strives to promote global collaboration in the field of materials science and technology. It primarily publishes original research papers, invited review articles, letters, research notes, and summaries of scientific achievements. The journal covers a wide range of materials science and technology topics, including metallic materials, inorganic nonmetallic materials, and composite materials.
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