In-melt electron analysis to accelerate process exploration of ceramics: Electron beam melting of TiB2

IF 3 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Materialia Pub Date : 2024-09-26 DOI:10.1016/j.mtla.2024.102243
Jinghao Xu , Karin Wennersten , Zongwen Fu , Freddy Leijon , Johan Moverare
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Abstract

To enhance the versatility of electron beam powder bed fusion (EB-PBF), a widely utilized additive manufacturing (AM) technique for metallic materials, we propose a novel paradigm aimed at facilitating the exploration of the process parameters for less-studied materials, such as ceramics. The high melting points and poorly understood thermal properties of ceramics have constrained the comprehension of their melting behavior. In this study, titanium diboride (TiB2) sintered bodies were subjected to spot melting under four distinct electron beam currents and four different exposure times. By introducing a novel in-melt electron analysis (IMEA) approach, the various stages of melting were clearly identified. The analysis and interpretation of IMEA signals were found to be consistent with experimental observations on the spot-melted surface of TiB2. IMEA demonstrates significant potential for real-time process window optimization and quality assurance for challenging and novel materials.

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熔融电子分析加速陶瓷工艺探索:电子束熔化 TiB2
电子束粉末床熔融(EB-PBF)是一种广泛应用于金属材料的增材制造(AM)技术,为了提高这种技术的多功能性,我们提出了一种新的范例,旨在促进对陶瓷等研究较少的材料的工艺参数的探索。陶瓷的高熔点和热特性鲜为人知,限制了对其熔化行为的理解。在这项研究中,二硼化钛(TiB2)烧结体在四种不同的电子束电流和四种不同的曝光时间下进行了点熔。通过引入新颖的熔融电子分析(IMEA)方法,清楚地识别了熔化的各个阶段。对 IMEA 信号的分析和解释与对 TiB2 点熔表面的实验观察结果一致。IMEA 在实时优化工艺窗口和保证具有挑战性的新型材料的质量方面展示了巨大的潜力。
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来源期刊
Materialia
Materialia MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
6.40
自引率
2.90%
发文量
345
审稿时长
36 days
期刊介绍: Materialia is a multidisciplinary journal of materials science and engineering that publishes original peer-reviewed research articles. Articles in Materialia advance the understanding of the relationship between processing, structure, property, and function of materials. Materialia publishes full-length research articles, review articles, and letters (short communications). In addition to receiving direct submissions, Materialia also accepts transfers from Acta Materialia, Inc. partner journals. Materialia offers authors the choice to publish on an open access model (with author fee), or on a subscription model (with no author fee).
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