Toward advanced analytical procedures for detecting Fumonisins in contaminated food and feed using molecularly imprinted polymers: A mini review

IF 4.9 2区化学 Q1 CHEMISTRY, ANALYTICAL Microchemical Journal Pub Date : 2024-10-10 DOI:10.1016/j.microc.2024.111858

M.A. Diab , Heba A. El-Sabban , Kwang-Hyun Baek

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Abstract

Fumonisins (FMS), a class of Mycotoxins mostly produced by fusarium species, are found in polluted food and feed and can seriously harm humans and animals. To ensure food safety and regulatory compliance, accurate and dependable analytical techniques are utilized in detecting and measuring these pollutants. This mini-review focused on sophisticated clean-up techniques for Fumonisin (FM) analysis utilizing molecularly imprinted polymer solid phase extraction (MIPSPE). The majority of the molecularly imprinted polymers (MIPs) categories that are intended to extract FMs from the food matrix were discussed, along with a list of well-known chromatographic techniques and MIP-based electrochemical sensors to detect FMs.

By imitating FM-specific natural sites, MIPSPE provides great selectivity, sensitivity, and reproducibility while improving the accuracy of subsequent analytical tests. This review includes the synthesis of MIPs, extraction protocol optimization, and integration with several detection techniques like High-Performance Liquid Chromatography (HPLC) and Liquid Chromatography-Mass Spectroscopy (LC-MS). It also covers recent advancements in MIPSPE technology.

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利用分子印迹聚合物开发检测受污染食品和饲料中伏马菌素的先进分析程序：微型综述

伏马菌毒素（FMS）是一类霉菌毒素，主要由镰刀菌产生，存在于受污染的食品和饲料中，会对人类和动物造成严重危害。为确保食品安全和符合法规要求，需要使用准确可靠的分析技术来检测和测量这些污染物。本微型综述重点介绍利用分子印迹聚合物固相萃取（MIPSPE）分析伏马菌毒素（FM）的复杂净化技术。通过模仿伏马菌毒素的特异性天然位点，MIPSPE 可提供极高的选择性、灵敏度和可重复性，同时提高后续分析测试的准确性。本综述包括 MIPs 的合成、萃取方案优化以及与多种检测技术的整合，如高效液相色谱法（HPLC）和液相色谱-质谱法（LC-MS）。报告还介绍了 MIPSPE 技术的最新进展。

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来源期刊

Microchemical Journal 化学-分析化学

CiteScore

8.70

自引率

8.30%

发文量

1131

审稿时长

1.9 months

期刊介绍： The Microchemical Journal is a peer reviewed journal devoted to all aspects and phases of analytical chemistry and chemical analysis. The Microchemical Journal publishes articles which are at the forefront of modern analytical chemistry and cover innovations in the techniques to the finest possible limits. This includes fundamental aspects, instrumentation, new developments, innovative and novel methods and applications including environmental and clinical field. Traditional classical analytical methods such as spectrophotometry and titrimetry as well as established instrumentation methods such as flame and graphite furnace atomic absorption spectrometry, gas chromatography, and modified glassy or carbon electrode electrochemical methods will be considered, provided they show significant improvements and novelty compared to the established methods.