Experimental and analytical study on the compressive behavior of PMI foam with different densities and cell sizes under intermediate strain rates

IF 5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Polymer Testing Pub Date : 2024-10-02 DOI:10.1016/j.polymertesting.2024.108593
Peilin Zhu, Jili Rong, Shenglong Wang, Zichao Chen
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Abstract

Polymethacrylimide (PMI) foam materials have great potential for applications in the field of protective energy absorption owing to their superior compressive properties. Existing studies on the mechanical behavior of PMI foams are limited, particularly for loading at intermediate strain rates. This paper presents a comprehensive experimental study of PMI foam with four different densities under quasi-static and intermediate strain rate compression (0.001 s−1 to 100 s−1). Each density included three different cell sizes to determine their effects on the compressive performance. Loads parallel and perpendicular to the foam rise direction were considered to investigate the anisotropic behavior. Intermediate strain rate tests were conducted using a high-speed hydraulic servo testing machine, which achieved a stable strain rate while ensuring consistent specimen sizes in both quasi-static and dynamic tests. In all the experiments, the compression process was captured using a high-speed camera and the macroscopic deformation mode and microscopic deformation mechanism were analyzed by combining Digital Image Correlation (DIC) and Scanning Electron Microscopy (SEM). The PMI foam with finer cell sizes exhibited an enhanced compression performance. As the strain rate increased, the strain rate effect became more evident in the high-density specimens and an increase in cell size diminished this effect. A modified analytical model incorporating the cell-size correction term was developed based on Gibson and Ashby's model. The modified model exhibited an average error of 4.9 % in the predicted plateau stress of PMI foam with different cell sizes at the same density.
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不同密度和单元尺寸的聚甲基丙烯酸甲酯泡沫在中等应变速率下的压缩行为的实验和分析研究
聚甲基丙烯酰亚胺(PMI)泡沫材料因其卓越的抗压性能,在保护性能量吸收领域具有巨大的应用潜力。现有关于聚甲基丙烯酰亚胺泡沫材料力学行为的研究非常有限,尤其是在中等应变速率下的加载。本文介绍了在准静态和中等应变率压缩(0.001 s-1 至 100 s-1)条件下对四种不同密度的 PMI 泡沫进行的综合实验研究。每种密度包括三种不同的孔径,以确定它们对压缩性能的影响。为了研究各向异性行为,还考虑了与泡沫上升方向平行和垂直的载荷。中间应变速率试验使用高速液压伺服试验机进行,该试验机可实现稳定的应变速率,同时确保准静态和动态试验中试样尺寸的一致性。在所有试验中,都使用高速相机拍摄了压缩过程,并结合数字图像相关性(DIC)和扫描电子显微镜(SEM)分析了宏观变形模式和微观变形机制。孔径更细的 PMI 泡沫的压缩性能更佳。随着应变速率的增加,应变速率效应在高密度试样中变得更加明显,而细胞尺寸的增加则减弱了这种效应。在 Gibson 和 Ashby 模型的基础上,开发了一个包含单元尺寸修正项的修正分析模型。修改后的模型显示,在相同密度下,不同细胞尺寸的 PMI 泡沫的预测高原应力平均误差为 4.9%。
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来源期刊
Polymer Testing
Polymer Testing 工程技术-材料科学:表征与测试
CiteScore
10.70
自引率
5.90%
发文量
328
审稿时长
44 days
期刊介绍: Polymer Testing focuses on the testing, analysis and characterization of polymer materials, including both synthetic and natural or biobased polymers. Novel testing methods and the testing of novel polymeric materials in bulk, solution and dispersion is covered. In addition, we welcome the submission of the testing of polymeric materials for a wide range of applications and industrial products as well as nanoscale characterization. The scope includes but is not limited to the following main topics: Novel testing methods and Chemical analysis • mechanical, thermal, electrical, chemical, imaging, spectroscopy, scattering and rheology Physical properties and behaviour of novel polymer systems • nanoscale properties, morphology, transport properties Degradation and recycling of polymeric materials when combined with novel testing or characterization methods • degradation, biodegradation, ageing and fire retardancy Modelling and Simulation work will be only considered when it is linked to new or previously published experimental results.
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