{"title":"Decreasing propagation rate of interfacial debonding between a single carbon fiber and epoxy matrix under cyclic loading","authors":"Kosuke Takahashi , Takuma Matsuo , Wataru Sato , Takashi Nakamura","doi":"10.1016/j.compscitech.2024.110900","DOIUrl":null,"url":null,"abstract":"<div><div>The interfacial debonding of a single carbon fiber transversely embedded in a dumbbell-shaped epoxy sample was generated under cyclic loading, and images were captured using synchrotron radiation X-ray computed tomography. A fatigue testing machine driven by a piezoelectric actuator placed along the beamline for <em>in situ</em> observation was developed for precise alignment. Interfacial debonding was initially observed under a static tensile load and was confirmed to be almost of the same length at both ends of the carbon fiber, implying negligible bending deformation due to inclination. Cyclic loads were then applied to the sample to capture the progressive debonding. The propagation rate of the interfacial debonding decreased as the number of cycles increased. Another sample with a single carbon fiber aligned parallel to the loading direction was prepared following a single-fiber fragmentation test. Interfacial debonding was clearly observed around the fiber breakage. Cyclic loads were also applied to this sample; however, no progression of the interfacial debonding was evident. Degradation of the interfacial strength between the carbon fiber and epoxy matrix was not confirmed under cyclic loading within the elastic deformation range.</div></div>","PeriodicalId":283,"journal":{"name":"Composites Science and Technology","volume":"258 ","pages":"Article 110900"},"PeriodicalIF":8.3000,"publicationDate":"2024-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Composites Science and Technology","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0266353824004706","RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, COMPOSITES","Score":null,"Total":0}
引用次数: 0
Abstract
The interfacial debonding of a single carbon fiber transversely embedded in a dumbbell-shaped epoxy sample was generated under cyclic loading, and images were captured using synchrotron radiation X-ray computed tomography. A fatigue testing machine driven by a piezoelectric actuator placed along the beamline for in situ observation was developed for precise alignment. Interfacial debonding was initially observed under a static tensile load and was confirmed to be almost of the same length at both ends of the carbon fiber, implying negligible bending deformation due to inclination. Cyclic loads were then applied to the sample to capture the progressive debonding. The propagation rate of the interfacial debonding decreased as the number of cycles increased. Another sample with a single carbon fiber aligned parallel to the loading direction was prepared following a single-fiber fragmentation test. Interfacial debonding was clearly observed around the fiber breakage. Cyclic loads were also applied to this sample; however, no progression of the interfacial debonding was evident. Degradation of the interfacial strength between the carbon fiber and epoxy matrix was not confirmed under cyclic loading within the elastic deformation range.
在循环载荷作用下,单根碳纤维横向嵌入哑铃形环氧树脂样品中,产生了界面脱粘现象,并利用同步辐射 X 射线计算机断层扫描捕捉到了图像。开发了一种由压电致动器驱动的疲劳试验机,沿光束线放置,用于原位观测,以实现精确对准。最初是在静态拉伸载荷下观察界面脱粘情况,结果证实碳纤维两端的长度几乎相同,这意味着倾斜导致的弯曲变形可以忽略不计。然后对样品施加循环载荷,以捕捉渐进式脱胶。随着循环次数的增加,界面脱粘的传播速度也在下降。在单根碳纤维破碎试验后,制备了另一个与加载方向平行的单根碳纤维样品。在纤维断裂周围明显观察到界面脱粘现象。对该样品也施加了循环载荷,但未发现界面脱粘现象。在弹性变形范围内施加循环载荷时,碳纤维和环氧基体之间的界面强度没有发生退化。
期刊介绍:
Composites Science and Technology publishes refereed original articles on the fundamental and applied science of engineering composites. The focus of this journal is on polymeric matrix composites with reinforcements/fillers ranging from nano- to macro-scale. CSTE encourages manuscripts reporting unique, innovative contributions to the physics, chemistry, materials science and applied mechanics aspects of advanced composites.
Besides traditional fiber reinforced composites, novel composites with significant potential for engineering applications are encouraged.