Ernesto Aguilar-Palazuelos, Perla Rosa Fitch-Vargas, Carlos Iván Delgado-Nieblas, Agustín López-Diaz, Aliette Gastélum-Ávila, Marco Antonio Sánchez-Chilero, Víctor Limón-Valenzuela, Irma Leticia Camacho-Hernández, Xóchitl Ariadna Ruiz-Armenta, Abraham Calderón-Castro
{"title":"Edible Films Based on Corn Starch and Gelatin Obtained by the Combination of Extrusion and Casting Process: Characterization and Applications","authors":"Ernesto Aguilar-Palazuelos, Perla Rosa Fitch-Vargas, Carlos Iván Delgado-Nieblas, Agustín López-Diaz, Aliette Gastélum-Ávila, Marco Antonio Sánchez-Chilero, Víctor Limón-Valenzuela, Irma Leticia Camacho-Hernández, Xóchitl Ariadna Ruiz-Armenta, Abraham Calderón-Castro","doi":"10.1007/s11483-024-09891-1","DOIUrl":null,"url":null,"abstract":"<div><p>The development of edible films (EFs) using renewable resources such as gelatin and native corn starch has garnered significant interest due to their potential to enhance food preservation and safety. Combining extrusion with the casting method enhances mechanical and barrier properties by modifying starch and gelatin structures through heat, pressure, and shear. This study aimed to develop, characterize, and optimize the functional properties EFs produced from an extruded formulation of corn starch, gelatin, and glycerol using the casting method. Furthermore, it evaluated the impact of these optimized EFs as coatings on the quality characteristics of the “Kent” mango cultivar. The study factors were gelatin content (GC, 0–10%) and extrusion temperature (ET, 80–120°C). The EFs were characterized and optimized, determining the tensile strength (<i>σ</i>), elongation (<i>ε</i>), water vapor permeability (WVP), and Water Solubility (S), using the surface response methodology. Results showed GC significantly influenced mechanical and barrier properties (<i>P <</i> 0.05), with higher GC increasing σ, ε, WVP, and S. ET also affected mechanical properties (<i>P <</i> 0.05) but not barrier properties (<i>P ></i> 0.05). EFs exhibited <i>σ</i> of 3.14 MPa to 8.34 MPa, <i>ε</i> of 10.55–25.60%, WVP (5.59 × 10<sup>–12</sup> to 6.82 × 10<sup>–11</sup> g m Pa<sup>-1</sup> s<sup>-1</sup> m<sup>-2</sup>), and S from 66.29–80.50%. According to the optimization study, the EFs with the best mechanical and barrier properties were obtained using an ET of 80°C and GC of 2.93%. Applied as coatings on ‘Kent’ mango, these EFs significantly extended shelf life and preserved postharvest quality.</p></div>","PeriodicalId":564,"journal":{"name":"Food Biophysics","volume":"20 1","pages":""},"PeriodicalIF":2.8000,"publicationDate":"2024-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Food Biophysics","FirstCategoryId":"97","ListUrlMain":"https://link.springer.com/article/10.1007/s11483-024-09891-1","RegionNum":4,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"FOOD SCIENCE & TECHNOLOGY","Score":null,"Total":0}
引用次数: 0
Abstract
The development of edible films (EFs) using renewable resources such as gelatin and native corn starch has garnered significant interest due to their potential to enhance food preservation and safety. Combining extrusion with the casting method enhances mechanical and barrier properties by modifying starch and gelatin structures through heat, pressure, and shear. This study aimed to develop, characterize, and optimize the functional properties EFs produced from an extruded formulation of corn starch, gelatin, and glycerol using the casting method. Furthermore, it evaluated the impact of these optimized EFs as coatings on the quality characteristics of the “Kent” mango cultivar. The study factors were gelatin content (GC, 0–10%) and extrusion temperature (ET, 80–120°C). The EFs were characterized and optimized, determining the tensile strength (σ), elongation (ε), water vapor permeability (WVP), and Water Solubility (S), using the surface response methodology. Results showed GC significantly influenced mechanical and barrier properties (P < 0.05), with higher GC increasing σ, ε, WVP, and S. ET also affected mechanical properties (P < 0.05) but not barrier properties (P > 0.05). EFs exhibited σ of 3.14 MPa to 8.34 MPa, ε of 10.55–25.60%, WVP (5.59 × 10–12 to 6.82 × 10–11 g m Pa-1 s-1 m-2), and S from 66.29–80.50%. According to the optimization study, the EFs with the best mechanical and barrier properties were obtained using an ET of 80°C and GC of 2.93%. Applied as coatings on ‘Kent’ mango, these EFs significantly extended shelf life and preserved postharvest quality.
期刊介绍:
Biophysical studies of foods and agricultural products involve research at the interface of chemistry, biology, and engineering, as well as the new interdisciplinary areas of materials science and nanotechnology. Such studies include but are certainly not limited to research in the following areas: the structure of food molecules, biopolymers, and biomaterials on the molecular, microscopic, and mesoscopic scales; the molecular basis of structure generation and maintenance in specific foods, feeds, food processing operations, and agricultural products; the mechanisms of microbial growth, death and antimicrobial action; structure/function relationships in food and agricultural biopolymers; novel biophysical techniques (spectroscopic, microscopic, thermal, rheological, etc.) for structural and dynamical characterization of food and agricultural materials and products; the properties of amorphous biomaterials and their influence on chemical reaction rate, microbial growth, or sensory properties; and molecular mechanisms of taste and smell.
A hallmark of such research is a dependence on various methods of instrumental analysis that provide information on the molecular level, on various physical and chemical theories used to understand the interrelations among biological molecules, and an attempt to relate macroscopic chemical and physical properties and biological functions to the molecular structure and microscopic organization of the biological material.