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Elucidating the Influence of Coating Materials in the Microencapsulation Process of Hempseed Oil Via Spray Drying: A Comprehensive Analysis of Physicochemical Attributes, Oxidation Stability, and Thermal Properties 阐明涂层材料在喷雾干燥法微胶囊化大麻籽油过程中的影响:理化属性、氧化稳定性和热性能的综合分析
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-27 DOI: 10.1007/s11483-024-09859-1
Kutlu Cevik, Hasan Yalcin, Yusuf Konca

In this study, it was aimed to investigate the effect of different coating materials on the microencapsulation of hempseed oil by spray drying. For this purpose, hempseed oil emulsions were prepared with skimmed milk powder (SMP), maltodextrin (MD), and whey protein concentrate (WPC). The properties of these emulsions including rheological, zeta potential, and physicochemical properties were analyzed. Then, hempseed oil microcapsules were produced using spray drying. The effect of the different coating materials on spray-dried hempseed oil capsules was evaluated in terms of microencapsulation yield, surface oil, microencapsulation efficiency, oxidation stability, and physicochemical properties. The combinations of SMP (50.58%) or WPC (56.21%) with MD significantly enhanced the microencapsulation yield. The highest microencapsulation efficiency (92.16%) was obtained in the microcapsule with SMP: MD. This microcapsule with SMP: MD also showed higher oxidative stability compared to other microcapsules. Besides, this combination (SMP: MD) effectively protected the hempseed oil against oxidation during the Schaal oven test. Additionally, spray-dried hempseed oil microcapsules were characterized using FT-IR, TGA, and SEM. It was determined that using MD as a coating material improved the thermal stability of the microcapsules. As a result, it was concluded that the SMP: MD as a coating material was suitable for the microencapsulation of hempseed oil.

本研究旨在探讨不同包衣材料对喷雾干燥法微囊化大麻籽油的影响。为此,用脱脂奶粉(SMP)、麦芽糊精(MD)和浓缩乳清蛋白(WPC)制备了大麻籽油乳剂。对这些乳液的流变学、ZETA电位和理化性质进行了分析。然后,采用喷雾干燥法生产了大麻籽油微胶囊。从微胶囊产量、表面油、微胶囊效率、氧化稳定性和理化性质等方面评估了不同包衣材料对喷雾干燥麻籽油胶囊的影响。将 SMP(50.58%)或 WPC(56.21%)与 MD 结合使用可显著提高微囊产量。SMP: MD 微胶囊的微胶囊效率最高(92.16%)。与其他微胶囊相比,SMP: MD 微胶囊的氧化稳定性也更高。此外,这种组合(SMP:MD)在沙尔炉试验中有效地保护了大麻籽油免受氧化。此外,还使用傅立叶变换红外光谱、热重分析和扫描电镜对喷雾干燥的大麻籽油微胶囊进行了表征。结果表明,使用 MD 作为涂层材料可提高微胶囊的热稳定性。因此,可以得出结论:以 MD 作为涂层材料的 SMP 适用于大麻籽油的微胶囊化。
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引用次数: 0
State Diagrams of Binary Mixtures of Saturated Monoglycerides in Vegetable and Mineral Oil and their Impact in the Oleogels Rheology 植物油和矿物油中饱和单甘酯二元混合物的状态图及其对油凝胶流变学的影响
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-24 DOI: 10.1007/s11483-024-09847-5
M. E. Charó-Alvarado, M. A. Charó-Alonso, J. F. Toro-Vazquez

State diagrams of binary mixtures of 1-stearoyl glycerol (C18) with 1-myristoyl glycerol (C14), 1-palmitoyl glycerol (C16) or 1-monobehenin glycerol (C22) in vegetable and mineral oil were obtained using different molar fractions of the monoglycerides (MGs) keeping the MG concentration constant (8% wt/wt). We observed that, independent of the MG mixture (C18:C14, C18:C16, C18:C22) and the type of oil, the MGs developed a mixed Lα phase with a transition temperature practically independent of the C18 molar fraction. In contrast, the transition temperature for the sub-α phase showed a eutectic point that, for the same MG mixture, occurred in both oils at the same MG molar fraction. At the MG molar composition corresponding to the eutectic point, the difference in length between the aliphatic chains in the mixed lamella resulted in a sub-α phase with the least efficient chain packing compared to that developed by any other MG molar fraction. Independent of the MG mixture and the type of oil, the oleogels developed by cooling (80 °C to 5 °C) followed by 180 min at 5 °C achieved the highest elasticity (G’5 °C) at the MG molar fraction composition associated with the eutectic point. Tentatively the least efficient aliphatic chains packing developed by the sub-α phase at the eutectic point, favored the incorporation and retention of higher amounts of oil. Thus, for a particular MG binary mixture, the oleogels at the eutectic point had the highest G’5 °C in comparison with the G’5 °C of oleogels formulated at any other MG proportion.

我们使用不同摩尔分数的单甘油酯(MGs)并保持 MG 浓度不变(8% wt/wt),得到了植物油和矿物油中 1-硬脂酰甘油(C18)与 1-肉豆蔻酰甘油(C14)、1-棕榈酰甘油(C16)或 1-单贝壳烯甘油(C22)的二元混合物的状态图。我们观察到,与 MG 混合物(C18:C14、C18:C16、C18:C22)和油的类型无关,MG 形成了混合 Lα 相,其转变温度实际上与 C18 摩尔分数无关。与此相反,亚α相的转变温度显示出一个共晶点,对于相同的 MG 混合物,在相同的 MG 摩尔分数下,两种油中都会出现该共晶点。在与共晶点相对应的 MG 摩尔成分中,混合薄片中脂肪族链的长度差异导致亚α相的链堆积效率比任何其他 MG 摩尔成分的亚α相都低。与 MG 混合物和油的类型无关,通过冷却(80 °C 至 5 °C)然后在 5 °C 下放置 180 分钟而形成的油凝胶在与共晶点相关的 MG 摩尔分数组成下获得了最高的弹性(G'5 °C)。在共晶点,亚α相形成的脂肪族链填料效率最低,这可能有利于掺入和保留更多的油。因此,对于特定的 MG 二元混合物,共晶点的油凝胶与任何其他 MG 比例配制的油凝胶相比,G'5 °C 最高。
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引用次数: 0
Value-added Applications of Fruit Peel Biowaste: A Review of Potential Uses in the Food Industry 果皮生物废料的增值应用:食品工业潜在用途综述
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-22 DOI: 10.1007/s11483-024-09845-7
Vonnie Merillyn Joseph, Kobun Rovina, Felicia Wen Xia Ling, Sarifah Supri, Koh Wee Yin

This review incorporates the appraisal of fruit peels, commonly dumped agro-waste, as a potential for developing value-added products and environmental issues. In Malaysia, the food industry uses fruits to produce various items ranging from fruit juices, concentrates, and jams to dried fruits that generate considerable organic waste. This inefficiency results in 25–30% of the total product content being discarded, primarily comprising peel wastes from fruits such as oranges, bananas, pomegranates, and lemons. These peels are especially rich in bioactive elements, including pigments, polyphenols, enzymes, vitamins and antioxidants. The review examines the technical interventions planned to produce compounds of high value using these compounds. By utilising different extraction methodologies, the peels' bioactive substances can be extracted. These methods require optimisation to get a maximum yield and a high purity of compounds. Extracted compounds are then utilised in the production of numerous products. The article highlights the potential of these compounds as an ingredient for creating food coatings, probiotics, natural antioxidants, natural dyes, and biosorbents. By changing this waste into cost-effective products, we can progress tremendously toward sustainable use and valorisation of biowaste. This review paper reviews the various fruit peels and their prospective uses, offering a new angle on waste management and resource utilisation in the food industry.

Graphical Abstract

本综述结合了对果皮(通常被倾倒的农业废弃物)的评估,认为其具有开发增值产品和解决环境问题的潜力。在马来西亚,食品工业利用水果生产各种产品,从果汁、浓缩果汁、果酱到干果,这些产品会产生大量有机废物。这种低效率导致总产品含量的 25-30% 被丢弃,主要是橘子、香蕉、石榴和柠檬等水果的果皮废物。这些果皮尤其富含生物活性元素,包括色素、多酚、酶、维生素和抗氧化剂。本综述探讨了利用这些化合物生产高价值化合物的技术干预计划。通过采用不同的提取方法,可以提取果皮中的生物活性物质。这些方法需要优化,以获得最高产量和高纯度的化合物。提取的化合物可用于生产多种产品。文章强调了这些化合物作为食品涂层、益生菌、天然抗氧化剂、天然染料和生物吸附剂原料的潜力。通过将这些废物转化为具有成本效益的产品,我们可以在生物废物的可持续利用和增值方面取得巨大进步。本文综述了各种果皮及其潜在用途,为食品工业的废物管理和资源利用提供了一个新的视角。
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引用次数: 0
Functional, Thermal, Pasting, and Antioxidant Properties of Flour from Indian Browntop Millet (Brachiaria ramosa) Cultivars 印度棕顶黍(Brachiaria ramosa)栽培品种面粉的功能、热、糊化和抗氧化特性
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-21 DOI: 10.1007/s11483-024-09858-2
Amisha Kaushik, Dharmesh Chandra Saxena, Sukhcharn Singh

The present study aimed to characterize the functional, morphological, thermal, pasting, rheological, and antioxidant properties of flour samples from Indian browntop millet cultivars. Significant (p < 0.05) difference was observed for various chemical constituents except crude fiber content. Water absorption (2.04–2.14) and Oil absorption capacity (2.25–2.35) varied significantly among cultivars. At 90 °C, BTM4 (6.59) and BTM1 (6.29) showed the highest and lowest swelling power. The DPPH assay and TPC analysis revealed the highest scavenging activity (51.24%) and phenolic content (3.24 mg GAE/g), exhibited by BTM2. Thermal analysis revealed distinct transition temperatures with onset temperatures ranging from 27.06 °C (BTM4) to 43.11 °C (BTM1). Peak viscosity values ranged from 381 cP (BTM4) to 703 cP (BTM2), while final viscosity values ranged from 726 cP (BTM4) to 1922 cP (BTM1), respectively. Steady and dynamic rheological tests demonstrated weak-gel-like behavior in all flour samples, with storage modulus (G’) exceeding loss modulus (G”). FT-IR analysis showed a broad intensity peak ranging between 3268.31 cm−1 to 3280.29 cm−1. SEM images depicted the granular microstructure, revealing spherical and irregular particles ranging from 2.34 μm to 12.4 μm across the cultivars. X-ray diffraction analysis revealed A-type crystallinity in all samples, with BTM4 exhibiting significantly higher relative crystallinity (25.54%). These findings highlight the diverse techno-functional characteristics of Indian Browntop millet flour and its potential as a valuable ingredient for enhancing various food formulations.

本研究旨在表征印度糙米种植品种面粉样品的功能、形态、热、糊化、流变和抗氧化特性。除粗纤维含量外,各种化学成分均存在显著差异(p < 0.05)。不同品种的吸水率(2.04-2.14)和吸油量(2.25-2.35)差异显著。90 °C 时,BTM4(6.59)和 BTM1(6.29)的膨胀力最高和最低。DPPH 分析和 TPC 分析表明,BTM2 的清除活性(51.24%)和酚含量(3.24 mg GAE/g)最高。热分析表明,起始温度在 27.06 ℃(BTM4)至 43.11 ℃(BTM1)之间,具有明显的转变温度。峰值粘度从 381 cP(BTM4)到 703 cP(BTM2)不等,最终粘度从 726 cP(BTM4)到 1922 cP(BTM1)不等。稳定和动态流变测试表明,所有面粉样品都具有弱凝胶状行为,储存模量(G')超过了损耗模量(G")。傅立叶变换红外光谱分析显示,在 3268.31 cm-1 至 3280.29 cm-1 之间有一个宽强度峰。扫描电子显微镜(SEM)图像显示了颗粒状的微观结构,不同品种的颗粒大小从 2.34 μm 到 12.4 μm 不等。X 射线衍射分析表明,所有样品都具有 A 型结晶度,其中 BTM4 的相对结晶度更高(25.54%)。这些发现凸显了印度棕顶小米粉的多种技术功能特性,以及其作为一种有价值的配料来改善各种食品配方的潜力。
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引用次数: 0
Identification of Potential α-Glucosidase Inhibitors from American Ginseng Processed Products by UHPLC-Q-Orbitrap/MS and Molecular Docking 通过超高效液相色谱-Q-轨道rap/质谱和分子对接鉴定西洋参加工产品中潜在的 α-葡萄糖苷酶抑制剂
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-18 DOI: 10.1007/s11483-024-09860-8
Liwen Liang, Xiaokang Liu, Juan Shao, Jiaqi Shen, Youzhen Yao, Xin Huang, Guangzhi Cai, Yunlong Guo, Jiyu Gong

The traditional herb American ginseng (Panax quinquefolium L.) can be processed into two common products: dried American ginseng (DAG) and red American ginseng (RAG), which have well-established hypoglycemic activity, making it a functional food as well. However, the mechanism by which the main active ingredients inhibit α-glucosidase, a crucial target for hypoglycemic drugs, remains unclear. In this research, we employed ultra-high-performance liquid chromatography coupled with quadrupole orbitrap mass spectrometry (UHPLC-Q-Orbitrap/MS) to analyze the chemical composition of ethanol extracts of dried American ginseng (EDAG) and red American ginseng (ERAG). Subsequent in vitro experiments were conducted to assess the α-glucosidase inhibitory activity of EDAG and ERAG. Comparative enzymatic kinetics analyses were performed as well. Molecular docking analysis revealed the interaction between the differential saponins and α-glucosidase, further validated through verification experiments. Among the total 47 identified saponins, 9 were characterized by OPLS-DA as differentially expressed between EDAG and ERAG. Notably, ERAG exhibited more robust α-glucosidase inhibitory activity than EDAG. Enzyme inhibition kinetics revealed that both products displayed reversible mixed-type inhibition on α-glucosidase, suggesting their inhibitory effects are associated with saponin composition. Molecular docking studies demonstrated that all 9 differential saponins exhibited inhibitory effects on α-glucosidase. Verification studies substantiated ginsenosides like Rb1, Rd, and others as inhibitors of α-glucosidase. These findings contribute to a more comprehensive understanding of processed American ginseng and provide valuable insights for developing glucose-lowering functional foods.

传统草药西洋参(Panax quinquefolium L.)可加工成两种常见产品:干西洋参(DAG)和红西洋参(RAG)。然而,其主要活性成分抑制α-葡萄糖苷酶(降糖药物的一个重要靶点)的机制仍不清楚。在这项研究中,我们采用超高效液相色谱-四极杆轨道质谱(UHPLC-Q-Orbitrap/MS)分析了干西洋参(EDAG)和红参(ERAG)乙醇提取物的化学成分。随后进行了体外实验,以评估 EDAG 和 ERAG 的 α-葡萄糖苷酶抑制活性。同时还进行了酶动力学对比分析。分子对接分析揭示了不同皂苷与 α-葡萄糖苷酶之间的相互作用,并通过验证实验进行了进一步验证。在总共鉴定出的 47 种皂甙中,有 9 种通过 OPLS-DA 鉴定出在 EDAG 和 ERAG 之间有差异表达。值得注意的是,ERAG 比 EDAG 表现出更强的α-葡萄糖苷酶抑制活性。酶抑制动力学显示,这两种产品都对α-葡萄糖苷酶有可逆的混合型抑制作用,表明它们的抑制作用与皂苷成分有关。分子对接研究表明,所有 9 种不同的皂苷都对α-葡萄糖苷酶有抑制作用。验证研究证实了 Rb1、Rd 等人参皂甙是 α-葡萄糖苷酶的抑制剂。这些发现有助于更全面地了解加工后的西洋参,并为开发降糖功能食品提供了宝贵的见解。
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引用次数: 0
Impact of Germination Treatment and Quinoa Variety on the Physicochemical and Rheological Properties of Wheat Dough 发芽处理和藜麦品种对小麦面团理化和流变特性的影响
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-15 DOI: 10.1007/s11483-024-09856-4
Luciano M Guardianelli, M. V. Salinas, M. C. Puppo
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引用次数: 0
Delivery of Curcumin Using Colloidal Complexes Formed from Ammonium Chitosan and Acid Treated Soybean Protein 利用壳聚糖铵和酸处理大豆蛋白形成的胶体复合物输送姜黄素
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-12 DOI: 10.1007/s11483-024-09855-5
Shuni Weng, Huanhuan Su, D. Mcclements, Yuting Wang, Teng Li, Yuying Fu
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引用次数: 0
The Effect of the Addition of Spirulina spp. on the Quality Properties, Health Benefits, and Sensory Evaluation of Green Tea Kombucha 添加螺旋藻对绿茶昆布茶质量特性、健康益处和感官评价的影响
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-10 DOI: 10.1007/s11483-024-09857-3
Hoai-Hieu Vo, Kim-Diep Tran, Loan Le-Thi, Ngoc-Nhi Nguyen-Thi, Tu Nguyen-Van, Thanh-Vy Dinh-Thi, The-Anh Pham, Tam Nguyen-Thi, Tu Vu-Thi
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引用次数: 0
Physical, colour, and mechanical properties of pearls (citrus caviar) from three finger lime (Citrus australasica) varieties: Implications for economic value, quality grading, and benchmarking 三个指柠檬(Citrus australasica)品种的珍珠(柑橘鱼子酱)的物理、颜色和机械特性:对经济价值、质量分级和基准的影响
IF 3 4区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-06-07 DOI: 10.1007/s11483-024-09848-4
J. Nastasi, Keely Rose Perry, Joel Andrew Abbott, Jade Mia King, Eleanor W. Hoffman
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引用次数: 0
Iron/zinc Alginates as Vehicles for Food Fortification with Enhanced Stability in Polyphenol-Rich Foods 作为食品强化剂载体的铁/锌藻酸盐可增强富含多酚食品的稳定性
IF 3 4区 农林科学 Q2 Agricultural and Biological Sciences Pub Date : 2024-06-05 DOI: 10.1007/s11483-024-09854-6
Jesper T.N. Knijnenburg, Neni Zulfa Nengsih, Pornnapa Kasemsiri, Prinya Chindaprasirt, Michael B. Zimmermann, Kaewta Jetsrisuparb

Food fortification with iron (Fe) and zinc (Zn) can effectively reduce deficiencies of these important micronutrients, but the reactivity of bioavailable Fe compounds in foods remains a challenge. Here, this problem was tackled by binding water-soluble Fe3+ and Zn2+ sources to alginate by ionotropic gelation, resulting in the formation of mixed Fe/Zn alginate beads. The dry beads were 0.8–1.4 mm in diameter and had Fe and Zn contents of up to 143 mg/g. Fourier transform infrared (FTIR) spectroscopy confirmed the successful binding of Fe3+ and Zn2+ with the carboxylic acid groups of alginate with preferential binding of Fe3+ over Zn2+. When added to difficult-to-fortify polyphenol-rich foods, the Fe alginate beads caused smaller color changes than water-soluble Fe sources, confirming that binding Fe3+ to alginate reduced its reactivity and improved its stability. Adding increasing amounts of Zn into the beads further improved color stability as evidenced by the lower ΔE values. The in vitro Fe solubility was 75–90% within 120 min at pH 1.0, independent of the Zn content, suggesting that the Fe from these structures is released in the stomach and available for absorption in the intestine. Their improved stability may make these Fe/Zn alginates attractive dual fortificants for difficult-to-fortify foods.

食品中添加铁(Fe)和锌(Zn)可有效减少这些重要微量营养素的缺乏,但食品中生物可利用的铁化合物的反应性仍然是一个挑战。为了解决这个问题,研究人员通过离子凝胶化将水溶性 Fe3+ 和 Zn2+ 源与海藻酸盐结合,形成了铁/锌混合的海藻酸盐珠。干珠直径为 0.8-1.4 毫米,铁和锌含量高达 143 毫克/克。傅立叶变换红外(FTIR)光谱证实,Fe3+ 和 Zn2+ 成功地与海藻酸的羧酸基团结合,Fe3+ 比 Zn2+ 优先结合。当添加到难以强化的富含多酚的食品中时,与水溶性铁源相比,海藻酸铁珠引起的颜色变化较小,这证实了将 Fe3+ 与海藻酸结合可降低其反应性并提高其稳定性。在珠子中添加越来越多的 Zn 可进一步提高颜色的稳定性,这一点从较低的ΔE 值中可以看出。在 pH 值为 1.0 的条件下,体外铁溶解度在 120 分钟内达到 75-90%,与锌含量无关。由于这些藻酸盐具有更高的稳定性,因此对于难以强化的食品来说,它们是具有吸引力的双重强化剂。
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引用次数: 0
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Food Biophysics
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