Biodegradable photocatalytic film based on chia seed mucilage (xylose, glucose, and methyl glucuronic acid polysaccharides) containing barberry extract and SnO2 nanoparticles

Shirin Forouzan , Sajad Pirsa , Abolfazl Alirezalu
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Abstract

In this study, chia seed mucilage (CSM) was extracted and used to prepare biodegradable film. The prepared film was modified with barberry extract (Ex) and tin oxide (SnO2) nanoparticles (NPs). According to the obtained results, barberry extract significantly increased the thickness of the film, while tin oxide nanoparticles affected the thickness very little. Adding nanoparticles to the film decreased both the tensile strength and flexibility of the film. Barberry extract increased the tensile strength and flexibility of the film. Barberry extract and tin oxide nanoparticles decreased the permeability to water vapor in the films. Barberry extract and tin oxide nanoparticles both increased the antioxidant property of the film. The addition of barberry extract and tin oxide nanoparticles significantly increased the antibacterial properties of the film against both Staphylococcus aureus and Escherichia coli bacteria. Physical connections and electrostatic interactions between composite components were confirmed by Fourier transform infrared (FTIR) spectra. The X-ray diffraction (XRD) results showed the positive effect of tin oxide nanoparticles in the formation of the crystal structure of the composite film. Additives of extract and nanoparticle increased the thermal stability of the film. The mucilage film with the highest percentage of tin oxide nanoparticles up to 50 % caused the photocatalytic degradation of methylene blue.
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基于奇异籽粘液(木糖、葡萄糖和甲基葡萄糖醛酸多糖)的可生物降解光催化薄膜,其中含有巴桑提取物和二氧化硒纳米颗粒
本研究提取了奇异籽粘液(CSM)并用于制备生物降解薄膜。在制备的薄膜上添加了巴桑子提取物(Ex)和氧化锡纳米颗粒(NPs)。结果表明,桑葚提取物明显增加了薄膜的厚度,而纳米氧化锡颗粒对薄膜厚度的影响很小。在薄膜中添加纳米粒子会降低薄膜的拉伸强度和柔韧性。桑葚提取物提高了薄膜的拉伸强度和柔韧性。桑葚提取物和纳米氧化锡粒子降低了薄膜的水蒸气渗透性。桑葚提取物和纳米氧化锡粒子都提高了薄膜的抗氧化性。添加了桑葚提取物和纳米氧化锡颗粒后,薄膜对金黄色葡萄球菌和大肠杆菌的抗菌性能明显提高。傅立叶变换红外光谱(FTIR)证实了复合成分之间的物理连接和静电作用。X 射线衍射(XRD)结果表明,氧化锡纳米粒子对复合薄膜晶体结构的形成具有积极作用。提取物和纳米颗粒的添加增加了薄膜的热稳定性。纳米氧化锡颗粒比例最高的粘液膜达到了 50%,可对亚甲蓝进行光催化降解。
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