Preparation and application of novel sorbents for in-tube solid-phase microextraction

IF 11.8 1区 化学 Q1 CHEMISTRY, ANALYTICAL Trends in Analytical Chemistry Pub Date : 2024-11-08 DOI:10.1016/j.trac.2024.118047
Feng Juanjuan, Ziyi Jiang, Yali Ding, Xiaomin Li, Min Sun
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Abstract

As the efficient sample preparation technique, in-tube solid-phase microextraction (SPME) was often combined with some analytical means containing chromatography or mass spectrometry for sensitive detection of various analytes. Especially, in-tube SPME-liquid chromatographic detection not only reduced the analytical time but also improved the accuracy of result. Moreover, this technique was environmentally friendly and employed minimal amount of organic solvents. Various sorbent materials and different extraction devices have been developed to improve enrichment efficiency. Four main types of extraction devices for in-tube SPME, including fiber-filled tube, monolithic column, sorbent-coated and particle-packed tubes, were reviewed from 2020 to 2024. Except for the preparation methods and new sorbents of these extraction devices, their applications in food analysis, environmental pollution and biomedical detection fields were also described. Additionally, the current challenges and future trends of in-tube SPME were discussed.
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管内固相微萃取新型吸附剂的制备与应用
作为一种高效的样品制备技术,管内固相微萃取(SPME)通常与一些包含色谱或质谱的分析手段相结合,用于灵敏地检测各种分析物。特别是管内固相微萃取-液相色谱检测,不仅缩短了分析时间,还提高了结果的准确性。此外,该技术对环境友好,使用的有机溶剂量极少。为了提高富集效率,人们开发了各种吸附剂材料和不同的萃取装置。从 2020 年到 2024 年,对管内 SPME 的四种主要萃取装置进行了回顾,包括纤维填充管、整体柱、吸附剂涂层管和颗粒包装管。除了介绍这些萃取装置的制备方法和新型吸附剂外,还介绍了它们在食品分析、环境污染和生物医学检测领域的应用。此外,还讨论了管内 SPME 目前面临的挑战和未来的发展趋势。
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来源期刊
Trends in Analytical Chemistry
Trends in Analytical Chemistry 化学-分析化学
CiteScore
20.00
自引率
4.60%
发文量
257
审稿时长
3.4 months
期刊介绍: TrAC publishes succinct and critical overviews of recent advancements in analytical chemistry, designed to assist analytical chemists and other users of analytical techniques. These reviews offer excellent, up-to-date, and timely coverage of various topics within analytical chemistry. Encompassing areas such as analytical instrumentation, biomedical analysis, biomolecular analysis, biosensors, chemical analysis, chemometrics, clinical chemistry, drug discovery, environmental analysis and monitoring, food analysis, forensic science, laboratory automation, materials science, metabolomics, pesticide-residue analysis, pharmaceutical analysis, proteomics, surface science, and water analysis and monitoring, these critical reviews provide comprehensive insights for practitioners in the field.
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