Improving parent-austenite twinned grain reconstruction using electron backscatter diffraction in low carbon austenite

IF 5.3 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Scripta Materialia Pub Date : 2024-11-19 DOI:10.1016/j.scriptamat.2024.116459
Ruth M. Birch, T. Ben Britton, Warren J. Poole
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Abstract

Thermomechanical controlled processing (TMCP) is widely used to optimize the final properties of high strength low alloy (HSLA) steels, via microstructure engineering. The room temperature microstructures are influenced by the high temperature austenite phase, and the austenite microstructure can be accessed by reconstruction using electron backscatter diffraction (EBSD) data of the final microstructure. A challenge for reconstruction of the parent austenite grain (PAG) microstructure and subsequent austenite grain size measurement is the presence of austenite-phase annealing twins, and we address this challenge with a new ‘re-sort’ algorithm. Our algorithm has been validated using the retained austenite regions (which were recovered via advanced pattern matching of EBSD patterns). We demonstrate that the re-sort algorithm improves the PAG reconstruction significantly, especially for the grain boundary network and correlation with other methods of grain size assessment and development of TMCP steels.

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利用电子反向散射衍射改进低碳奥氏体中母体-奥氏体孪晶的重构
热机械控制加工(TMCP)被广泛用于通过微结构工程优化高强度低合金钢(HSLA)的最终性能。室温微观结构受高温奥氏体相的影响,奥氏体微观结构可通过使用最终微观结构的电子反向散射衍射(EBSD)数据进行重构来获得。奥氏体相退火孪晶的存在是重构母体奥氏体晶粒(PAG)微观结构和后续奥氏体晶粒尺寸测量所面临的一个挑战,我们采用了一种新的 "重新分选 "算法来应对这一挑战。我们使用保留的奥氏体区域(通过 EBSD 图形的高级模式匹配恢复)验证了我们的算法。我们证明了重新排序算法显著改善了 PAG 重建,尤其是在晶界网络以及与其他晶粒度评估方法的相关性和 TMCP 钢的开发方面。
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来源期刊
Scripta Materialia
Scripta Materialia 工程技术-材料科学:综合
CiteScore
11.40
自引率
5.00%
发文量
581
审稿时长
34 days
期刊介绍: Scripta Materialia is a LETTERS journal of Acta Materialia, providing a forum for the rapid publication of short communications on the relationship between the structure and the properties of inorganic materials. The emphasis is on originality rather than incremental research. Short reports on the development of materials with novel or substantially improved properties are also welcomed. Emphasis is on either the functional or mechanical behavior of metals, ceramics and semiconductors at all length scales.
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