Enhancing Wear Resistance in Glass Ionomer Cement through Green-mediated Chitosan-, Titanium-, Zirconium-, and Hydroxyapatite-based Nanocomposites: An Analysis before and after Chewing Simulator Endurance.

Q3 Dentistry International Journal of Clinical Pediatric Dentistry Pub Date : 2024-11-01 Epub Date: 2024-12-19 DOI:10.5005/jp-journals-10005-2984
Srinavasa Surya Sitaram, Jessy Paulraj, Subhabrata Maiti, Rajeshkumar Shanmugam
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Abstract

Aim and background: Glass ionomer cement (GIC) serves as a widely used restorative dental material, known for its direct bonding to tooth structures and fluoride-releasing properties. This study aims to investigate the enhancement of GIC through the incorporation of a green-mediated nanocomposite comprising chitosan, titanium, zirconium, and hydroxyapatite, with a focus on evaluating the wear resistance of the modified GIC.

Materials and methods: A one-pot synthesis technique was utilized to prepare a green-mediated nanocomposite incorporating chitosan, titanium, zirconium, and hydroxyapatite nanoparticles. Forty extracted teeth fulfilling the inclusion criteria were chosen for the study. Each tooth received a class I cavity preparation, and then they were divided into groups. Each group, comprising 10 teeth, received a restoration using green-mediated nanocomposite-modified GIC in varying concentrations: 3% for group I, 5% for group II, and 10% for group III. Additionally, there was a control group (group IV) consisting of conventional GIC without any modifications. To assess the wear resistance of the samples, they underwent a testing protocol, followed by placement in a chewing simulator for 30,000 cycles. Surface scans before and after chewing simulation were conducted, and deviations were superimposed using Geomagic software. The interim of root mean square (RMS), maximum deviation, and average deviation were analyzed to quantify the wear levels. Then the data obtained were subjected to statistical analysis, one-way analysis of variance (ANOVA), followed by Tukey's post hoc analysis to identify any significant differences among the groups.

Results: The least deviation of RMS (0.292 ± 0.063), maximum deviation (0.664 ± 0.076), and average deviation (0.263 ± 0.049) were observed in the 5% nanocomposite-based GIC group, followed by the 10 and 3% groups. The nanocomposite-modified GIC groups exhibited superior wear resistance compared to the conventional group. This outcome addressed the limitations of traditional GIC, signifying a substantial advancement in dental restorative solutions.

Conclusion: The incorporation of green-mediated chitosan, titanium, zirconium, and hydroxyapatite nanocomposite into GIC demonstrated a remarkable improvement in wear resistance. This study paves the way for future advancements in dental materials, representing a significant stride toward the creation of environmentally conscious and efficacious dental restorations.

How to cite this article: Sitaram SS, Paulraj J, Maiti S, et al. Enhancing Wear Resistance in Glass Ionomer Cement through Green-mediated Chitosan-, Titanium-, Zirconium-, and Hydroxyapatite-based Nanocomposites: An Analysis before and after Chewing Simulator Endurance. Int J Clin Pediatr Dent 2024;17(11):1229-1235.

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绿色介导的壳聚糖、钛、锆和羟基磷灰石纳米复合材料增强玻璃离聚体水泥的耐磨性:咀嚼模拟器耐力前后的分析。
目的与背景:玻璃离子水门合剂(GIC)是一种广泛使用的牙齿修复材料,以其直接与牙齿结构结合和释放氟化物的特性而闻名。本研究旨在研究由壳聚糖、钛、锆和羟基磷灰石组成的绿色介导纳米复合材料对GIC的增强作用,并重点评估改性GIC的耐磨性。材料与方法:采用一锅合成技术制备了壳聚糖、钛、锆和羟基磷灰石纳米颗粒的绿色介导纳米复合材料。选择符合纳入标准的拔牙40颗进行研究。每颗牙齿接受I类空腔预备,然后分成组。每组包括10颗牙齿,使用不同浓度的绿色介导的纳米复合材料修饰的GIC进行修复:第一组为3%,第二组为5%,第三组为10%。此外,还有一个对照组(IV组),由常规GIC组成,不作任何修改。为了评估样品的耐磨性,他们接受了一项测试方案,然后在咀嚼模拟器中放置了30,000个循环。模拟咀嚼前后进行表面扫描,并用Geomagic软件进行偏差叠加。通过分析均方根(RMS)、最大偏差和平均偏差的中间值来量化磨损程度。然后对获得的数据进行统计分析、单因素方差分析(ANOVA),然后进行Tukey事后分析,以确定组间是否存在显著差异。结果:5%纳米复合材料GIC组的RMS偏差最小(0.292±0.063),最大偏差(0.664±0.076),平均偏差(0.263±0.049),其次为10%和3%组。与常规组相比,纳米复合材料修饰的GIC组具有更好的耐磨性。这一结果解决了传统GIC的局限性,标志着牙齿修复解决方案的实质性进步。结论:绿色介导的壳聚糖、钛、锆和羟基磷灰石纳米复合材料掺入GIC后,其耐磨性显著提高。这项研究为未来牙科材料的发展铺平了道路,代表了向创造环保意识和有效的牙科修复迈出了重要的一步。文章出处:Sitaram SS, Paulraj J, Maiti S,等。绿色介导的壳聚糖、钛、锆和羟基磷灰石纳米复合材料增强玻璃离聚体水泥的耐磨性:咀嚼模拟器耐力前后的分析。中华临床儿科杂志;2017;17(11):1229-1235。
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