Production of α–Al2O3–3YSZ Porous Ceramics with α(γ)–Al2O3 Additive

IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CERAMICS Glass and Ceramics Pub Date : 2025-01-11 DOI:10.1007/s10717-025-00713-5
Yu. I. Komolikov, L. V. Ermakova, R. A. Shishkin, V. M. Skachkov, V. D. Zhuravlev
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Abstract

α–Al2O3–3YSZ porous ceramics were fabricated using the slip casting method with the incorporation of 15 wt% of submicron Al2O3 powders as sintering additives. The materials were prepared by solution combustion synthesis using glycine or urea as fuels. Following firing of the ceramics at 1550°C, the percentage of closed porosity was found to be in the range from 14.1 to 24.0%. The experimental results revealed a linear correlation between density and closed porosity of Al2O3–3YSZ corundum ceramics. Ceramic samples that underwent firing at 1550°C exhibited relative density values ranging from 75 to 85%, accompanied by an open porosity of 0.90 to 1.71%. The findings indicate that the morphology of the used aluminum oxide additives synthesized through combustion exerts a predominant influence on the strength characteristics.

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α(γ) -Al2O3添加剂制备α -Al2O3 - 3ysz多孔陶瓷
采用滑移浇铸法制备α-Al2O3-3YSZ多孔陶瓷,并添加15%亚微米Al2O3粉末作为烧结助剂。以甘氨酸或尿素为燃料,采用溶液燃烧合成法制备了该材料。经1550℃烧制后,封闭孔隙率在14.1% ~ 24.0%之间。实验结果表明,Al2O3-3YSZ刚玉陶瓷的密度与封闭孔隙率呈线性相关。在1550℃下烧制的陶瓷样品的相对密度值在75 ~ 85%之间,孔隙率为0.90 ~ 1.71%。结果表明,燃烧合成的助剂的形貌对助剂的强度特性有重要影响。
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来源期刊
Glass and Ceramics
Glass and Ceramics 工程技术-材料科学:硅酸盐
CiteScore
1.00
自引率
16.70%
发文量
85
审稿时长
6-12 weeks
期刊介绍: Glass and Ceramics reports on advances in basic and applied research and plant production techniques in glass and ceramics. The journal''s broad coverage includes developments in the areas of silicate chemistry, mineralogy and metallurgy, crystal chemistry, solid state reactions, raw materials, phase equilibria, reaction kinetics, physicochemical analysis, physics of dielectrics, and refractories, among others.
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