The contribution of γ' phase transition induced (PI-CDRX) - CDRX-DDRX alternating cycling behavior to the hot formability of GH4079 alloy

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-02-01 Epub Date: 2024-12-31 DOI:10.1016/j.matchar.2024.114710
Xiaojie Zhang , Chengchuang Tao , Ge Zhou , Haoyu Zhang , Siqian Zhang , Xin Ma , Bin Gan , Lijia Chen
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Abstract

The hot deformation behavior of nickel-based superalloys at different temperatures (1025–1150 °C) and different strain rates (0.001–1 s−1) was studied by isothermal hot compression experiments using a Gleeble-3800 thermal simulator. According to the obtained stress-strain curve, the Arrhenius constitutive model based on the phase transition temperature segmentation was established. The correlation coefficient and the average absolute error were 0.992 and 0.978, respectively. Based on the thermal processing theory, the thermal processing maps based on Prassad, Gegel, Murty and Malas instability criteria were constructed and the rheological instability conditions of materials were predicted. The microstructure nucleation mechanism of DRX was studied by scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). The results show that due to the strong pinning effect of γ' phase on grain boundaries and the interaction between γ' phase and dislocations, the hot deformation behavior of the material at the phase transition temperature (1067 °C) is significantly different. The PI-CDRX (γ' phase-induced continuous dynamic recrystallization) and CDRX (continuous dynamic recrystallization) mechanisms dominate below the phase transition temperature. The DRX mechanism above the transformation temperature is mainly DDRX (discontinuous dynamic recrystallization), and the degree of DRX gradually increases with the increase of the deformation temperature. In addition, the ∑3 twin boundaries contribute to the nucleation of DRX grains.
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γ′相变诱导(PI-CDRX) - CDRX-DDRX交变循环行为对GH4079合金热成形性能的影响
采用Gleeble-3800热模拟装置,研究了镍基高温合金在不同温度(1025 ~ 1150℃)和不同应变速率(0.001 ~ 1 s−1)下的热压缩行为。根据得到的应力应变曲线,建立了基于相变温度分割的Arrhenius本构模型。相关系数为0.992,平均绝对误差为0.978。基于热加工理论,构建了基于Prassad、Gegel、Murty和Malas不稳定判据的热加工图,并对材料流变不稳定条件进行了预测。采用扫描电镜(SEM)、电子背散射衍射(EBSD)和透射电镜(TEM)研究了DRX的微观结构成核机理。结果表明:由于γ′相对晶界的强钉钉作用以及γ′相与位错的相互作用,材料在相变温度(1067℃)下的热变形行为存在显著差异;在相变温度以下,PI-CDRX (γ′相诱导连续动态再结晶)和CDRX(连续动态再结晶)机制占主导地位。相变温度以上的DRX机制主要为DDRX(不连续动态再结晶),DRX程度随变形温度的升高而逐渐增大。另外,∑3孪晶界有利于DRX晶粒的形核。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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